1,3,2',6'-tetraazido-3',4'-dideoxy-3'-enoneamine

Base Information

Chemical Name:1,3,2',6'-tetraazido-3',4'-dideoxy-3'-enoneamine
CAS No.:860640-70-6
Molecular Formula:C₁₂H₁₆N₁₂O₄
Molecular Weight:392.337
Hs Code.:

Synonyms:1,3,2',6'-tetraazido-3',4'-dideoxy-3'-enoneamine

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Chemical Property of 1,3,2',6'-tetraazido-3',4'-dideoxy-3'-enoneamine

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Technology Process of 1,3,2',6'-tetraazido-3',4'-dideoxy-3'-enoneamine

There total 5 articles about 1,3,2',6'-tetraazido-3',4'-dideoxy-3'-enoneamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 860640-71-7
C₁₈H₂₄N₁₂O₄

: 860640-70-6
1,3,2',6'-tetraazido-3',4'-dideoxy-3'-enoneamine

Guidance literature:: With acetic acid; In 1,4-dioxane; water; at 65 ℃; for 24h;
DOI:10.1081/CAR-200059968

Reference yield: 49.0%

: 688744-65-2
1,3,2’,6’-tetrazido-5,6-O-cyclohexylidene neamine

: 860640-70-6
1,3,2',6'-tetraazido-3',4'-dideoxy-3'-enoneamine

: 860640-71-7
C₁₈H₂₄N₁₂O₄

Guidance literature:: 1,3,2’,6’-tetrazido-5,6-O-cyclohexylidene neamine; With pyridine; trifluoromethylsulfonic anhydride; In dichloromethane;

With sodium thiosulfate; sodium iodide; In acetone;

Reference yield:

: 1053694-75-9
C₂₀H₂₄F₆N₁₂O₁₀S₂

: 860640-70-6
1,3,2',6'-tetraazido-3',4'-dideoxy-3'-enoneamine

Guidance literature:: Multi-step reaction with 2 steps

1: 0.39 g / sodium iodide; sodium thiosulfate / acetone / 20 °C

2: 95 percent / acetic acid / H₂O; dioxane / 24 h / 65 °C

With sodium thiosulfate; acetic acid; sodium iodide; In 1,4-dioxane; water; acetone;
DOI:10.1081/CAR-200059968