(5R,6S,E)-5-(3-tert-butyldimethylsilyloxypropyl)-2-(2'-(methoxymethoxy)ethylidene)-6-(phenylsulfonyl)cyclohex-3-enone

Base Information

Chemical Name:(5R,6S,E)-5-(3-tert-butyldimethylsilyloxypropyl)-2-(2'-(methoxymethoxy)ethylidene)-6-(phenylsulfonyl)cyclohex-3-enone
CAS No.:1341190-79-1
Molecular Formula:C₂₅H₃₈O₆SSi
Molecular Weight:494.725
Hs Code.:

Synonyms:(5R,6S,E)-5-(3-tert-butyldimethylsilyloxypropyl)-2-(2'-(methoxymethoxy)ethylidene)-6-(phenylsulfonyl)cyclohex-3-enone

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Chemical Property of (5R,6S,E)-5-(3-tert-butyldimethylsilyloxypropyl)-2-(2'-(methoxymethoxy)ethylidene)-6-(phenylsulfonyl)cyclohex-3-enone

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Technology Process of (5R,6S,E)-5-(3-tert-butyldimethylsilyloxypropyl)-2-(2'-(methoxymethoxy)ethylidene)-6-(phenylsulfonyl)cyclohex-3-enone

There total 1 articles about (5R,6S,E)-5-(3-tert-butyldimethylsilyloxypropyl)-2-(2'-(methoxymethoxy)ethylidene)-6-(phenylsulfonyl)cyclohex-3-enone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₂H₂₄O₂Si

: 1341190-59-7
(E)-5-(methoxymethoxy)-1-(phenylsulfonyl)pent-3-en-2-one

: (5R,6S,Z)-5-(3-tert-butyldimethylsilyloxypropyl)-2-(2'-(methoxymethoxy)ethylidene)-6-(phenylsulfonyl)cyclohex-3-enone

: 1341190-79-1
(5R,6S,E)-5-(3-tert-butyldimethylsilyloxypropyl)-2-(2'-(methoxymethoxy)ethylidene)-6-(phenylsulfonyl)cyclohex-3-enone

Guidance literature:: C₁₂H₂₄O₂Si; (E)-5-(methoxymethoxy)-1-(phenylsulfonyl)pent-3-en-2-one; With (S)-2-{bis[3,5-bis(trifluoromethyl)phenyl][(trimethylsilanyl)oxy]methyl}pyrrolidine; In chloroform-d1; for 30h;

With L-proline; In chloroform-d1; for 115h; optical yield given as %ee; enantioselective reaction;
DOI:10.1016/j.tet.2011.08.068