6'-N,4'-O-carbonyl-4'',6''-O-cyclohexylidene-3'-deoxy-2''-O-(imidazolylthiocarbonyl)-5,2'-O-isopropylidene-1,3,3''-tri-N-tosylkanamycin A

Base Information

Chemical Name:6'-N,4'-O-carbonyl-4'',6''-O-cyclohexylidene-3'-deoxy-2''-O-(imidazolylthiocarbonyl)-5,2'-O-isopropylidene-1,3,3''-tri-N-tosylkanamycin A
CAS No.:78150-56-8
Molecular Formula:C₅₃H₆₆N₆O₁₇S₄
Molecular Weight:1187.4
Hs Code.:

Synonyms:6'-N,4'-O-carbonyl-4'',6''-O-cyclohexylidene-3'-deoxy-2''-O-(imidazolylthiocarbonyl)-5,2'-O-isopropylidene-1,3,3''-tri-N-tosylkanamycin A

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Chemical Property of 6'-N,4'-O-carbonyl-4'',6''-O-cyclohexylidene-3'-deoxy-2''-O-(imidazolylthiocarbonyl)-5,2'-O-isopropylidene-1,3,3''-tri-N-tosylkanamycin A

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Technology Process of 6'-N,4'-O-carbonyl-4'',6''-O-cyclohexylidene-3'-deoxy-2''-O-(imidazolylthiocarbonyl)-5,2'-O-isopropylidene-1,3,3''-tri-N-tosylkanamycin A

There total 1 articles about 6'-N,4'-O-carbonyl-4'',6''-O-cyclohexylidene-3'-deoxy-2''-O-(imidazolylthiocarbonyl)-5,2'-O-isopropylidene-1,3,3''-tri-N-tosylkanamycin A which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 78150-55-7
6'-N,4'-O-carbonyl-4'',6''-O-cyclohexylidene-3',2''-bis-O-(imidazolylthiocarbonyl)-5,2'-O-isopropylidene-1,3,3''-tri-N-tosylkanamycin A

: 78150-56-8
6'-N,4'-O-carbonyl-4'',6''-O-cyclohexylidene-3'-deoxy-2''-O-(imidazolylthiocarbonyl)-5,2'-O-isopropylidene-1,3,3''-tri-N-tosylkanamycin A

Guidance literature:: With tri-n-butyl-tin hydride; In tetrahydrofuran; at 110 ℃; for 3h;
DOI:10.1016/S0008-6215(00)85232-5

Reference yield:

: 78150-56-8
6'-N,4'-O-carbonyl-4'',6''-O-cyclohexylidene-3'-deoxy-2''-O-(imidazolylthiocarbonyl)-5,2'-O-isopropylidene-1,3,3''-tri-N-tosylkanamycin A

: 6'-N,4'-O-carbonyl-4'',6''-O-cyclohexylidene-3',2''-dideoxy-5,2'-O-isopropylidene-1,3,3''-tri-N-tosylkanamycin A

: 78150-57-9
6'-N,4'-O-carbonyl-4'',6''-O-cyclohexylidene-3'-deoxy-5,2'-O-isopropylidene-1,3,3''-tri-N-tosylkanamycin A

Guidance literature:: With ammonium hydroxide; ethanol; In tetrahydrofuran; for 5h; Ambient temperature;
DOI:10.1016/S0008-6215(00)85232-5

Reference yield:

: 78150-56-8
6'-N,4'-O-carbonyl-4'',6''-O-cyclohexylidene-3'-deoxy-2''-O-(imidazolylthiocarbonyl)-5,2'-O-isopropylidene-1,3,3''-tri-N-tosylkanamycin A

: 78822-39-6
3'-deoxykanamycin A monocarbonate

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / 28 percent aq. NH₃, ethanol / tetrahydrofuran / 5 h / Ambient temperature

2: 80 percent aq. acetic acid / 1.5 h / 80 °C

With ammonium hydroxide; ethanol; acetic acid; In tetrahydrofuran;
DOI:10.1016/S0008-6215(00)85232-5