3-O-(3,4,6-tri-O-acetyl-2-amino-2-deoxy-α-D-galactopyranosyl)-N-(benzyloxycarbonyl)-L-serine methyl ester

Base Information

Chemical Name:3-O-(3,4,6-tri-O-acetyl-2-amino-2-deoxy-α-D-galactopyranosyl)-N-(benzyloxycarbonyl)-L-serine methyl ester
CAS No.:74084-37-0
Molecular Formula:C₂₄H₃₂N₂O₁₂
Molecular Weight:540.524
Hs Code.:

Synonyms:3-O-(3,4,6-tri-O-acetyl-2-amino-2-deoxy-α-D-galactopyranosyl)-N-(benzyloxycarbonyl)-L-serine methyl ester

Suppliers and Price of 3-O-(3,4,6-tri-O-acetyl-2-amino-2-deoxy-α-D-galactopyranosyl)-N-(benzyloxycarbonyl)-L-serine methyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-O-(3,4,6-tri-O-acetyl-2-amino-2-deoxy-α-D-galactopyranosyl)-N-(benzyloxycarbonyl)-L-serine methyl ester

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of 3-O-(3,4,6-tri-O-acetyl-2-amino-2-deoxy-α-D-galactopyranosyl)-N-(benzyloxycarbonyl)-L-serine methyl ester

There total 8 articles about 3-O-(3,4,6-tri-O-acetyl-2-amino-2-deoxy-α-D-galactopyranosyl)-N-(benzyloxycarbonyl)-L-serine methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 74084-36-9
3-O-(3,4,6-tri-O-acetyl-2-azido-2-deoxy-α-D-galactopyranosyl)-N-(benzyloxycarbonyl)-L-serine methyl ester

: 74084-37-0
3-O-(3,4,6-tri-O-acetyl-2-amino-2-deoxy-α-D-galactopyranosyl)-N-(benzyloxycarbonyl)-L-serine methyl ester

Guidance literature:: With hydrogen; palladium on activated charcoal; In methanol; for 3h; under 760 Torr;
DOI:10.1016/S0008-6215(00)85142-3

Reference yield:

: 67817-37-2
3,4,6-tri-O-acetyl-2-azido-2-deoxy-β-D-galactopyranosyl chloride

: 74084-37-0
3-O-(3,4,6-tri-O-acetyl-2-amino-2-deoxy-α-D-galactopyranosyl)-N-(benzyloxycarbonyl)-L-serine methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) 4 Angstroem molecular sieve, 2.) mercuric cyanide, mercuric chloride / 1.) 30 min, nitromethane; 2.) nitromethane, 12 h, 70 deg C

2: 500 mg / H₂ / 5 percent Pd/C / methanol / 3 h / 760 Torr

With 4 A molecular sieve; hydrogen; mercury(II) cyanide; mercury dichloride; palladium on activated charcoal; In methanol;
DOI:10.1016/S0008-6215(00)85142-3

Reference yield:

: 1676-81-9
N-benzyloxycarbonyl-L-serine methyl ester

: 74084-37-0
3-O-(3,4,6-tri-O-acetyl-2-amino-2-deoxy-α-D-galactopyranosyl)-N-(benzyloxycarbonyl)-L-serine methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) 4 Angstroem molecular sieve, 2.) mercuric cyanide, mercuric chloride / 1.) 30 min, nitromethane; 2.) nitromethane, 12 h, 70 deg C

2: 500 mg / H₂ / 5 percent Pd/C / methanol / 3 h / 760 Torr

With 4 A molecular sieve; hydrogen; mercury(II) cyanide; mercury dichloride; palladium on activated charcoal; In methanol;
DOI:10.1016/S0008-6215(00)85142-3