(1RS,3SR,5RS,7SR)-8-[(4-methylphenyl)sulfonylyl]-4-oxa-8-azatricyclo[5.1.0.0^3,5]octane

Base Information

• Chemical Name: (1RS,3SR,5RS,7SR)-8-[(4-methylphenyl)sulfonylyl]-4-oxa-8-azatricyclo[5.1.0.0^3,5]octane
• CAS No.: 220555-54-4
• Molecular Formula: C₁₃H₁₅NO₃S
• Molecular Weight: 265.333

Synonyms:(1RS,3SR,5RS,7SR)-8-[(4-methylphenyl)sulfonylyl]-4-oxa-8-azatricyclo[5.1.0.0^3,5]octane

Chemical Property of (1RS,3SR,5RS,7SR)-8-[(4-methylphenyl)sulfonylyl]-4-oxa-8-azatricyclo[5.1.0.0^3,5]octane

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Technology Process of (1RS,3SR,5RS,7SR)-8-[(4-methylphenyl)sulfonylyl]-4-oxa-8-azatricyclo[5.1.0.0^3,5]octane

There total 2 articles about (1RS,3SR,5RS,7SR)-8-[(4-methylphenyl)sulfonylyl]-4-oxa-8-azatricyclo[5.1.0.0^3,5]octane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

7-[(4-methylphenyl)sulfonyl]-7-azabicyclo[4.1.0]hept-3-ene (112297-29-7) → (1RS,3SR,5RS,7SR)-8-[(4-methylphenyl)sulfonylyl]-4-oxa-8-azatricyclo[5.1.0.03,5]octane (220555-54-4) + (1RS,3RS,5SR,7SR)-8-[(4-methylphenyl)sulfonylyl]-4-oxa-8-azatricyclo[5.1.0.03,5]octane (220555-55-5)

Guidance literature:

With sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 20 ℃; for 16h; Further Variations:; Reagents; Solvents; Temperatures; time; Product distribution;

DOI:10.1039/b210608f

Reference yield:

7-(4-Methylphenylsulfonyl)-7-azabicyclo<4.1.0>hept-3-en (112297-29-7) → (1RS,3SR,5RS,7SR)-8-[(4-methylphenyl)sulfonylyl]-4-oxa-8-azatricyclo[5.1.0.03,5]octane (220555-54-4) + (1RS,3RS,5SR,7SR)-8-[(4-methylphenyl)sulfonylyl]-4-oxa-8-azatricyclo[5.1.0.03,5]octane (220555-55-5)

Guidance literature:

With sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; for 20h; Product distribution; Ambient temperature; variation of conditions; further epoxidations of cycloalkenes;

DOI:10.1016/S0040-4039(98)02320-X

Reference yield: 90.0%

(1RS,3SR,5RS,7SR)-8-[(4-methylphenyl)sulfonylyl]-4-oxa-8-azatricyclo[5.1.0.03,5]octane (220555-54-4) → N-((1R,2R,4S,5S)-4-Hydroxy-6,7-dithia-bicyclo[3.2.1]oct-2-yl)-4-methyl-benzenesulfonamide

Guidance literature:

With benzyltriethylammonium tetrathiomolybdate; In ethanol; acetonitrile; at 28 ℃; for 12h;

DOI:10.1021/ja052969z

upstream raw materials:

7-(4-Methylphenylsulfonyl)-7-azabicyclo<4.1.0>hept-3-en

7-[(4-methylphenyl)sulfonyl]-7-azabicyclo[4.1.0]hept-3-ene

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