N-(3-chloro-1,4-dioxo-1,4-dihydronaphthalen-2-yl)-cyclohexanesulfonamide

Base Information

Chemical Name:N-(3-chloro-1,4-dioxo-1,4-dihydronaphthalen-2-yl)-cyclohexanesulfonamide
CAS No.:1610042-45-9
Molecular Formula:C₁₆H₁₆ClNO₄S
Molecular Weight:353.826
Hs Code.:

Synonyms:N-(3-chloro-1,4-dioxo-1,4-dihydronaphthalen-2-yl)-cyclohexanesulfonamide

Suppliers and Price of N-(3-chloro-1,4-dioxo-1,4-dihydronaphthalen-2-yl)-cyclohexanesulfonamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of N-(3-chloro-1,4-dioxo-1,4-dihydronaphthalen-2-yl)-cyclohexanesulfonamide

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of N-(3-chloro-1,4-dioxo-1,4-dihydronaphthalen-2-yl)-cyclohexanesulfonamide

There total 2 articles about N-(3-chloro-1,4-dioxo-1,4-dihydronaphthalen-2-yl)-cyclohexanesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 117-80-6
2,3-Dichloro-1,4-naphthoquinone

: 2438-38-2
cyclohexanesulfonamide

: 1610042-45-9
N-(3-chloro-1,4-dioxo-1,4-dihydronaphthalen-2-yl)-cyclohexanesulfonamide

Guidance literature:: With caesium carbonate; In N,N-dimethyl-formamide; at 20 ℃; Sealed tube; Microwave irradiation;
DOI:10.1016/j.bmc.2014.03.015

Reference yield:

: 4837-38-1
cyclohexanesulfonyl chloride

: 1610042-45-9
N-(3-chloro-1,4-dioxo-1,4-dihydronaphthalen-2-yl)-cyclohexanesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1: ammonium hydroxide; hydrogenchloride / water / 1.67 h / 20 °C / pH 7

2: caesium carbonate / N,N-dimethyl-formamide / 20 °C / Sealed tube; Microwave irradiation

With hydrogenchloride; ammonium hydroxide; caesium carbonate; In water; N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2014.03.015