[1,1'-biphenyl]-4-carbaldehyde-α-d₁

Base Information

Chemical Name:[1,1'-biphenyl]-4-carbaldehyde-α-d₁
CAS No.:59151-15-4
Molecular Formula:C₁₃H₁₀O
Molecular Weight:183.214
Hs Code.:

[1,1'-biphenyl]-4-carbaldehyde-α-d<sub>1</sub>

Synonyms:[1,1'-biphenyl]-4-carbaldehyde-α-d₁

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of [1,1'-biphenyl]-4-carbaldehyde-α-d₁

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Technology Process of [1,1'-biphenyl]-4-carbaldehyde-α-d₁

There total 1 articles about [1,1'-biphenyl]-4-carbaldehyde-α-d₁ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 917-71-5
deuterated formic acid

: 1591-31-7
4-iodo-biphenyl

: 59151-15-4
[1,1'-biphenyl]-4-carbaldehyde-α-d₁

: 3218-36-8
4-Phenylbenzaldehyde

Guidance literature:: deuterated formic acid; 4-iodo-biphenyl; With palladium diacetate; acetic anhydride; tricyclohexylphosphine; In N,N-dimethyl-formamide; at 30 ℃; for 1h; Inert atmosphere; Green chemistry;

With triethylamine; In N,N-dimethyl-formamide; at 80 ℃; for 6h; Inert atmosphere; Green chemistry;
DOI:10.1002/chem.201600387

Reference yield:

: 59151-15-4
[1,1'-biphenyl]-4-carbaldehyde-α-d₁

: 13826-27-2
2,2'-bis(1,3,2-benzodioxaborole)

: C₁₉H₁₄⁽²⁾HBO₂

Guidance literature:: With water; In N,N-dimethyl acetamide; at 80 ℃; for 8h; chemoselective reaction; Inert atmosphere; Sealed tube;
DOI:10.1021/jacs.0c03813

Reference yield:

: 59151-15-4
[1,1'-biphenyl]-4-carbaldehyde-α-d₁

: 2-([1,1'-biphenyl]-4-ylmethyl-d)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Guidance literature:: Multi-step reaction with 2 steps

1: water / N,N-dimethyl acetamide / 8 h / 80 °C / Inert atmosphere; Sealed tube

2: triethylamine / N,N-dimethyl acetamide; water / 1 h / 20 °C

With water; triethylamine; In N,N-dimethyl acetamide; water;
DOI:10.1021/jacs.0c03813