C₃₅H₃₆N₆O₈S₂

Base Information

Chemical Name:C₃₅H₃₆N₆O₈S₂
CAS No.:1391396-74-9
Molecular Formula:C₃₅H₃₆N₆O₈S₂
Molecular Weight:732.838
Hs Code.:

C<sub>35</sub>H<sub>36</sub>N<sub>6</sub>O<sub>8</sub>S<sub>2</sub>

Synonyms:C₃₅H₃₆N₆O₈S₂

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Chemical Property of C₃₅H₃₆N₆O₈S₂

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Technology Process of C₃₅H₃₆N₆O₈S₂

There total 22 articles about C₃₅H₃₆N₆O₈S₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 1391396-68-1
C₁₃H₁₀BrNO₄

: 1391396-48-7
C₂₂H₂₉N₅O₅S₂

: 1391396-74-9
C₃₅H₃₆N₆O₈S₂

Guidance literature:: C₁₃H₁₀BrNO₄; C₂₂H₂₉N₅O₅S₂; With potassium hydrogencarbonate; In 1,2-dimethoxyethane; at 20 ℃; for 16h; Inert atmosphere;

With pyridine; trifluoroacetic anhydride; In 1,2-dimethoxyethane; at 0 ℃; for 3h; Inert atmosphere;

With triethylamine; In 1,2-dimethoxyethane; at 20 ℃; for 3h; Inert atmosphere;
DOI:10.1016/j.tetlet.2012.05.105

Reference yield:

: C₁₇H₃₀N₂O₆

: 1391396-74-9
C₃₅H₃₆N₆O₈S₂

Guidance literature:: Multi-step reaction with 13 steps

1.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / dichloromethane / 0.25 h / -20 °C / Inert atmosphere

1.2: 12 h / -20 - 20 °C / Inert atmosphere

2.1: lithium hydroxide / methanol; dichloromethane / 8 h / 20 °C

2.2: pH 1 / Acidic conditions

3.1: O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine / dichloromethane / 0.75 h / 20 °C / Inert atmosphere

4.1: palladium 10% on activated carbon; hydrogen / ethanol

5.1: diethylamino-sulfur trifluoride / dichloromethane / 1 h / -78 °C / Inert atmosphere

6.1: potassium carbonate / dichloromethane / -78 - 20 °C / Inert atmosphere

7.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / dichloromethane / 0.25 h / -20 °C / Inert atmosphere

7.2: 12 h / -20 - 20 °C / Inert atmosphere

8.1: ammonium hydroxide / methanol; water / 20 °C / Sonication

9.1: Lawessons reagent / 1,2-dimethoxyethane / 60 °C / Inert atmosphere

10.1: potassium hydrogencarbonate / 1,2-dimethoxyethane / 16 h / 20 °C / Inert atmosphere

10.2: 3 h / 0 °C / Inert atmosphere

10.3: 3 h / 20 °C / Inert atmosphere

11.1: ammonium hydroxide / methanol; water / 20 °C / Sonication

12.1: Lawessons reagent / 1,2-dimethoxyethane / 60 °C / Inert atmosphere

13.1: potassium hydrogencarbonate / 1,2-dimethoxyethane / 16 h / 20 °C / Inert atmosphere

13.2: 3 h / 0 °C / Inert atmosphere

13.3: 3 h / 20 °C / Inert atmosphere

With Lawessons reagent; ammonium hydroxide; diethylamino-sulfur trifluoride; palladium 10% on activated carbon; hydrogen; potassium carbonate; potassium hydrogencarbonate; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; 1,8-diazabicyclo[5.4.0]undec-7-ene; N-ethyl-N,N-diisopropylamine; lithium hydroxide; In methanol; 1,2-dimethoxyethane; ethanol; dichloromethane; water; 10.1: Hantzsch thiazole synthesis / 10.2: Hantzsch thiazole synthesis / 10.3: Hantzsch thiazole synthesis / 13.1: Hantzsch thiazole synthesis / 13.2: Hantzsch thiazole synthesis / 13.3: Hantzsch thiazole synthesis;
DOI:10.1016/j.tetlet.2012.05.105

Reference yield:

: C₁₆H₂₆N₂O₆

: 1391396-74-9
C₃₅H₃₆N₆O₈S₂

Guidance literature:: Multi-step reaction with 11 steps

1.1: O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine / dichloromethane / 0.75 h / 20 °C / Inert atmosphere

2.1: palladium 10% on activated carbon; hydrogen / ethanol

3.1: diethylamino-sulfur trifluoride / dichloromethane / 1 h / -78 °C / Inert atmosphere

4.1: potassium carbonate / dichloromethane / -78 - 20 °C / Inert atmosphere

5.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / dichloromethane / 0.25 h / -20 °C / Inert atmosphere

5.2: 12 h / -20 - 20 °C / Inert atmosphere

6.1: ammonium hydroxide / methanol; water / 20 °C / Sonication

7.1: Lawessons reagent / 1,2-dimethoxyethane / 60 °C / Inert atmosphere

8.1: potassium hydrogencarbonate / 1,2-dimethoxyethane / 16 h / 20 °C / Inert atmosphere

8.2: 3 h / 0 °C / Inert atmosphere

8.3: 3 h / 20 °C / Inert atmosphere

9.1: ammonium hydroxide / methanol; water / 20 °C / Sonication

10.1: Lawessons reagent / 1,2-dimethoxyethane / 60 °C / Inert atmosphere

11.1: potassium hydrogencarbonate / 1,2-dimethoxyethane / 16 h / 20 °C / Inert atmosphere

11.2: 3 h / 0 °C / Inert atmosphere

11.3: 3 h / 20 °C / Inert atmosphere

With Lawessons reagent; ammonium hydroxide; diethylamino-sulfur trifluoride; palladium 10% on activated carbon; hydrogen; potassium carbonate; potassium hydrogencarbonate; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; 1,8-diazabicyclo[5.4.0]undec-7-ene; N-ethyl-N,N-diisopropylamine; In methanol; 1,2-dimethoxyethane; ethanol; dichloromethane; water; 8.1: Hantzsch thiazole synthesis / 8.2: Hantzsch thiazole synthesis / 8.3: Hantzsch thiazole synthesis / 11.1: Hantzsch thiazole synthesis / 11.2: Hantzsch thiazole synthesis / 11.3: Hantzsch thiazole synthesis;
DOI:10.1016/j.tetlet.2012.05.105