N-acetyl-N'benzyl-N'-cyclopropylethylenediamine

Base Information

• Chemical Name: N-acetyl-N'benzyl-N'-cyclopropylethylenediamine
• CAS No.: 126105-21-3
• Molecular Formula: C₁₄H₂₀N₂O
• Molecular Weight: 232.326
• Mol file: 126105-21-3.mol

Synonyms:N-acetyl-N'benzyl-N'-cyclopropylethylenediamine

Chemical Property of N-acetyl-N'benzyl-N'-cyclopropylethylenediamine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N-acetyl-N'benzyl-N'-cyclopropylethylenediamine

There total 1 articles about N-acetyl-N'benzyl-N'-cyclopropylethylenediamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-benzyl-N-cyclopropylethylenediamine (91907-31-2) → N-acetyl-N'benzyl-N'-cyclopropylethylenediamine (126105-21-3)

Guidance literature:

With acetic anhydride;

Reference yield:

N-acetyl-N'benzyl-N'-cyclopropylethylenediamine (126105-21-3) → 4-Amino-5-chloro-N-[2-(cyclopropyl-ethyl-amino)-ethyl]-2-methoxy-benzamide

Guidance literature:

Multi-step reaction with 4 steps

1: 100 percent / H₂, HCl / 5percent Pd/C / ethanol / 2 h / Ambient temperature

2: potassium carbonate / dimethylformamide / 0.25 h / 80 °C

3: 15percent aq. HCl / 2 h / Heating

4: tetrahydrofuran / 1 h / 50 °C

With hydrogenchloride; hydrogen; potassium carbonate; palladium on activated charcoal; In tetrahydrofuran; ethanol; N,N-dimethyl-formamide;

DOI:10.1016/0223-5234(93)90129-3

Reference yield:

N-acetyl-N'benzyl-N'-cyclopropylethylenediamine (126105-21-3) → 4-Amino-5-chloro-N-[2-(cyclopropyl-isopropyl-amino)-ethyl]-2-methoxy-benzamide (126105-20-2)

Guidance literature:

Multi-step reaction with 4 steps

1: 100 percent / H₂, HCl / 5percent Pd/C / ethanol / 2 h / Ambient temperature

2: potassium carbonate / dimethylformamide / 0.25 h / 80 °C

3: 15percent aq. HCl / 2 h / Heating

4: tetrahydrofuran / 1 h / 50 °C

With hydrogenchloride; hydrogen; potassium carbonate; palladium on activated charcoal; In tetrahydrofuran; ethanol; N,N-dimethyl-formamide;

DOI:10.1016/0223-5234(93)90129-3

upstream raw materials:

N-benzyl-N-cyclopropylethylenediamine

Downstream raw materials:

N-benzyl-N-cyclopropylethylenediamine

N'-cyclopropylethane-1,2-diamine

N-cyclopropyl-N-methylethylenediamine

N¹-Cyclopropyl-N¹-ethyl-ethane-1,2-diamine