11-((bis(4-methoxyphenyl)(phenyl)methoxy)methyl)-4,4,6a,6b,8a,11,14b-heptamethyl-1,2,3,4,4a,5,6,6a,6b,7,8,8a,9,10,11,12,12a,14,14a,14b-eicosahydro-picen-3-ol

Base Information

• Chemical Name: 11-((bis(4-methoxyphenyl)(phenyl)methoxy)methyl)-4,4,6a,6b,8a,11,14b-heptamethyl-1,2,3,4,4a,5,6,6a,6b,7,8,8a,9,10,11,12,12a,14,14a,14b-eicosahydro-picen-3-ol
• CAS No.: 1159588-37-0
• Molecular Formula: C₅₁H₆₈O₄
• Molecular Weight: 745.099

Synonyms:11-((bis(4-methoxyphenyl)(phenyl)methoxy)methyl)-4,4,6a,6b,8a,11,14b-heptamethyl-1,2,3,4,4a,5,6,6a,6b,7,8,8a,9,10,11,12,12a,14,14a,14b-eicosahydro-picen-3-ol

Chemical Property of 11-((bis(4-methoxyphenyl)(phenyl)methoxy)methyl)-4,4,6a,6b,8a,11,14b-heptamethyl-1,2,3,4,4a,5,6,6a,6b,7,8,8a,9,10,11,12,12a,14,14a,14b-eicosahydro-picen-3-ol

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Technology Process of 11-((bis(4-methoxyphenyl)(phenyl)methoxy)methyl)-4,4,6a,6b,8a,11,14b-heptamethyl-1,2,3,4,4a,5,6,6a,6b,7,8,8a,9,10,11,12,12a,14,14a,14b-eicosahydro-picen-3-ol

There total 1 articles about 11-((bis(4-methoxyphenyl)(phenyl)methoxy)methyl)-4,4,6a,6b,8a,11,14b-heptamethyl-1,2,3,4,4a,5,6,6a,6b,7,8,8a,9,10,11,12,12a,14,14a,14b-eicosahydro-picen-3-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4,4'-dimethoxytrityl chloride (40615-36-9) + 11-hydroxymethyl-4,4a,6a,6b,8a,11,14b-heptamethyl-1,2,3,4,4a,5,6,6a,6b,7,8,8a,9,10,11,12,12a,14,14a,14b-eicosahydropicen-3-ol (6813-59-8) → 11-((bis(4-methoxyphenyl)(phenyl)methoxy)methyl)-4,4,6a,6b,8a,11,14b-heptamethyl-1,2,3,4,4a,5,6,6a,6b,7,8,8a,9,10,11,12,12a,14,14a,14b-eicosahydro-picen-3-ol (1159588-37-0)

Guidance literature:

With dmap; In pyridine; at 45 - 50 ℃; for 2h;

DOI:10.1016/j.tetlet.2009.03.049

Reference yield: 81.0%

11-((bis(4-methoxyphenyl)(phenyl)methoxy)methyl)-4,4,6a,6b,8a,11,14b-heptamethyl-1,2,3,4,4a,5,6,6a,6b,7,8,8a,9,10,11,12,12a,14,14a,14b-eicosahydro-picen-3-ol (1159588-37-0) + 2-cyanoethyl-N,N-(diisopropylamino)chlorophosphine (124482-92-4,89992-70-1) → 11-((bis(4-methoxyphenyl)(phenyl)methoxy)methyl)-4,4,6a,6b,8a,11,14b-heptamethyl-1,2,3,4,4a,5,6,6a,6b,7,8,8a,9,10,11,12,12a,14,14a,14b-eicosahydropicen-3-yl 2-cyanoethyl diisopropylphosphoramidite (1159588-38-1)

Guidance literature:

With 4-methyl-morpholine; In dichloromethane; at 20 ℃; for 0.0833333h;

DOI:10.1016/j.tetlet.2009.03.049

upstream raw materials:

4,4'-dimethoxytrityl chloride

11-hydroxymethyl-4,4a,6a,6b,8a,11,14b-heptamethyl-1,2,3,4,4a,5,6,6a,6b,7,8,8a,9,10,11,12,12a,14,14a,14b-eicosahydropicen-3-ol

Downstream raw materials:

11-((bis(4-methoxyphenyl)(phenyl)methoxy)methyl)-4,4,6a,6b,8a,11,14b-heptamethyl-1,2,3,4,4a,5,6,6a,6b,7,8,8a,9,10,11,12,12a,14,14a,14b-eicosahydropicen-3-yl 2-cyanoethyl diisopropylphosphoramidite

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