Benzoic acid (1R,3R,6S)-3-amino-6-hydroxy-cycloheptyl ester; hydrochloride

Base Information

Chemical Name:Benzoic acid (1R,3R,6S)-3-amino-6-hydroxy-cycloheptyl ester; hydrochloride
CAS No.:95687-94-8
Molecular Formula:C₁₄H₁₉NO₃*ClH
Molecular Weight:285.771
Hs Code.:

Synonyms:Benzoic acid (1R,3R,6S)-3-amino-6-hydroxy-cycloheptyl ester; hydrochloride

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Benzoic acid (1R,3R,6S)-3-amino-6-hydroxy-cycloheptyl ester; hydrochloride

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Technology Process of Benzoic acid (1R,3R,6S)-3-amino-6-hydroxy-cycloheptyl ester; hydrochloride

There total 4 articles about Benzoic acid (1R,3R,6S)-3-amino-6-hydroxy-cycloheptyl ester; hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 95687-89-1,95782-70-0
exo-3-(benzoyloxy)-8-oxa-9-azabicyclo<3.2.2.>-non-6-ene hydrochloride

: 95687-94-8
all-cis-5-amino-3-(benzoyloxy)cycloheptanol hydrochloride

Guidance literature:: With hydrogen; palladium on activated charcoal; In methanol; for 7h;
DOI:10.1021/jo00211a006

Reference yield:

: 59171-91-4
cyclohepta-3,5-dien-1-yl benzoate

: 95687-94-8
all-cis-5-amino-3-(benzoyloxy)cycloheptanol hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: 57 percent / ethanol; CCl₄ / 1.) -20 deg C, 5 h, 2.) -10 deg C, 14 d

2: 98 percent / H₂ / 5percent Pd/C / methanol / 7 h

With hydrogen; palladium on activated charcoal; In methanol; tetrachloromethane; ethanol;
DOI:10.1021/jo00211a006