C₂₉H₂₁N₃OS₃

Base Information

• Chemical Name: C₂₉H₂₁N₃OS₃
• CAS No.: 1616428-65-9
• Molecular Formula: C₂₉H₂₁N₃OS₃
• Molecular Weight: 523.703
• Mol file: 1616428-65-9.mol

Synonyms:C₂₉H₂₁N₃OS₃

Chemical Property of C₂₉H₂₁N₃OS₃

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₉H₂₁N₃OS₃

There total 9 articles about C₂₉H₂₁N₃OS₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

C30H23N3OS3 (1616428-64-8) → C29H21N3OS3 (1616428-65-9)

Guidance literature:

With boron tribromide; In dichloromethane; at -78 - 20 ℃;

DOI:10.1039/c4cc02179g

Reference yield:

5-methyl-2-phenyl-4-(2-phenylthiazol-4-yl)thiazole (1616428-67-1) → C29H21N3OS3 (1616428-65-9)

Guidance literature:

Multi-step reaction with 3 steps

1: N-Bromosuccinimide / N,N-dimethyl-formamide / 70 °C

2: cesium fluoride; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,4-dioxane / Inert atmosphere; Reflux

3: boron tribromide / dichloromethane / -78 - 20 °C

With N-Bromosuccinimide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; boron tribromide; cesium fluoride; In 1,4-dioxane; dichloromethane; N,N-dimethyl-formamide;

DOI:10.1039/c4cc02179g

Reference yield:

2,3-Pentanedione (600-14-6) → C29H21N3OS3 (1616428-65-9)

Guidance literature:

Multi-step reaction with 5 steps

1: bromine / 1.5 h / 20 °C

2: methanol / 0.33 h / 20 °C / Reflux

3: N-Bromosuccinimide / N,N-dimethyl-formamide / 70 °C

4: cesium fluoride; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,4-dioxane / Inert atmosphere; Reflux

5: boron tribromide / dichloromethane / -78 - 20 °C

With N-Bromosuccinimide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; bromine; boron tribromide; cesium fluoride; In 1,4-dioxane; methanol; dichloromethane; N,N-dimethyl-formamide;

DOI:10.1039/c4cc02179g

upstream raw materials:

1,4-dibromopentane-2,3-dione

5-methyl-2-phenyl-4-(2-phenylthiazol-4-yl)thiazole

5-bromo-5’-methyl-4,4’-bi-(2-phenyl)-thiazole

2,3-Pentanedione

Downstream raw materials:

C₄₁H₄₄N₆O₄S₃Si

C₃₂H₂₃N₃OS₃