3-(3-{2-[3-(3-hydroxy-2,2-dimethylpropyl)phenyl][1,3]dithian-2-yl}phenyl)-2,2-dimethylpropan-1-ol

Base Information

Chemical Name:3-(3-{2-[3-(3-hydroxy-2,2-dimethylpropyl)phenyl][1,3]dithian-2-yl}phenyl)-2,2-dimethylpropan-1-ol
CAS No.:413628-19-0
Molecular Formula:C₂₆H₃₆O₂S₂
Molecular Weight:444.703
Hs Code.:

Synonyms:3-(3-{2-[3-(3-hydroxy-2,2-dimethylpropyl)phenyl][1,3]dithian-2-yl}phenyl)-2,2-dimethylpropan-1-ol

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Chemical Property of 3-(3-{2-[3-(3-hydroxy-2,2-dimethylpropyl)phenyl][1,3]dithian-2-yl}phenyl)-2,2-dimethylpropan-1-ol

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Technology Process of 3-(3-{2-[3-(3-hydroxy-2,2-dimethylpropyl)phenyl][1,3]dithian-2-yl}phenyl)-2,2-dimethylpropan-1-ol

There total 4 articles about 3-(3-{2-[3-(3-hydroxy-2,2-dimethylpropyl)phenyl][1,3]dithian-2-yl}phenyl)-2,2-dimethylpropan-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 413628-17-8
3-(3-{2-[3-(2-ethoxycarbonyl-2-methylpropyl)phenyl][1,3]dithian-2-yl}phenyl)-2,2-dimethylpropionic acid ethyl ester

: 413628-19-0
3-(3-{2-[3-(3-hydroxy-2,2-dimethylpropyl)phenyl][1,3]dithian-2-yl}phenyl)-2,2-dimethylpropan-1-ol

Guidance literature:: With methanol; lithium borohydride; In dichloromethane; for 6h; Heating;
DOI:10.1021/jm040006p

Reference yield: 85.0%

: ammonium chloride

: 413628-17-8
3-(3-{2-[3-(2-ethoxycarbonyl-2-methylpropyl)phenyl][1,3]dithian-2-yl}phenyl)-2,2-dimethylpropionic acid ethyl ester

: 413628-19-0
3-(3-{2-[3-(3-hydroxy-2,2-dimethylpropyl)phenyl][1,3]dithian-2-yl}phenyl)-2,2-dimethylpropan-1-ol

Guidance literature:: With lithium borohydride; In methanol; dichloromethane;

Reference yield:

: 67660-38-2
3,3'-Bis(bromomethyl)benzophenone

: 413628-19-0
3-(3-{2-[3-(3-hydroxy-2,2-dimethylpropyl)phenyl][1,3]dithian-2-yl}phenyl)-2,2-dimethylpropan-1-ol

Guidance literature:: Multi-step reaction with 3 steps

1.1: LDA / tetrahydrofuran / 1 h / -78 °C

1.2: 89 percent / N,N'-dimethylpropyleneurea / tetrahydrofuran / 1 h / -78 - 20 °C

2.1: 87 percent / BF₃*Et₂O / CH₂Cl₂ / 20 °C

3.1: 85 percent / LiBH₄; MeOH / CH₂Cl₂ / 6 h / Heating

With methanol; lithium borohydride; boron trifluoride diethyl etherate; lithium diisopropyl amide; In tetrahydrofuran; dichloromethane;
DOI:10.1021/jm040006p