(C₁₃H₇OC₆H₆C₄H₈C₆H₄)2C₁₃H₆C₁₂H₂₆

Base Information

Chemical Name:(C₁₃H₇OC₆H₆C₄H₈C₆H₄)2C₁₃H₆C₁₂H₂₆
CAS No.:849222-41-9
Molecular Formula:C₈₃H₈₂O₂
Molecular Weight:1111.56
Hs Code.:

(C<sub>13</sub>H<sub>7</sub>OC<sub>6</sub>H<sub>6</sub>C<sub>4</sub>H<sub>8</sub>C<sub>6</sub>H<sub>4</sub>)2C<sub>13</sub>H<sub>6</sub>C<sub>12</sub>H<sub>26</sub>

Synonyms:(C₁₃H₇OC₆H₆C₄H₈C₆H₄)2C₁₃H₆C₁₂H₂₆

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Chemical Property of (C₁₃H₇OC₆H₆C₄H₈C₆H₄)2C₁₃H₆C₁₂H₂₆

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Technology Process of (C₁₃H₇OC₆H₆C₄H₈C₆H₄)2C₁₃H₆C₁₂H₂₆

There total 4 articles about (C₁₃H₇OC₆H₆C₄H₈C₆H₄)2C₁₃H₆C₁₂H₂₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 849222-39-5
C₁₃H₇OBrC₆H₆C₄H₈

: 849222-41-9
(C₁₃H₇OC₆H₆C₄H₈C₆H₄)2C₁₃H₆C₁₂H₂₆

Guidance literature:: Multi-step reaction with 2 steps

1: 61 percent / MeSO₃H / CH₂Cl₂ / 0.08 h / 20 °C

2: 1.96 g / hexaethylguanidinium chloride; K₂CO₃ / Pd(PPh₃)4 / toluene / 23 h / Heating

With methanesulfonic acid; hexaethylguanidinium chloride; potassium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In dichloromethane; toluene; 2: Suzuki coupling;
DOI:10.1021/ma0518353

Reference yield:

: 486-25-9,952573-42-1
9-fluorenone

: 849222-41-9
(C₁₃H₇OC₆H₆C₄H₈C₆H₄)2C₁₃H₆C₁₂H₂₆

Guidance literature:: Multi-step reaction with 4 steps

1.1: 71 percent / MeSO₃H; N-bromosuccinimide / Heating

2.1: Mg; 1,2-dibromoethane

2.2: 72 percent / diethyl ether / 1 h / Heating

3.1: 61 percent / MeSO₃H / CH₂Cl₂ / 0.08 h / 20 °C

4.1: 1.96 g / hexaethylguanidinium chloride; K₂CO₃ / Pd(PPh₃)4 / toluene / 23 h / Heating

With N-Bromosuccinimide; methanesulfonic acid; hexaethylguanidinium chloride; potassium carbonate; magnesium; ethylene dibromide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In dichloromethane; toluene; 4.1: Suzuki coupling;
DOI:10.1021/ma0518353

Reference yield:

: 3096-56-8
2-bromofluoren-9-one

: 849222-41-9
(C₁₃H₇OC₆H₆C₄H₈C₆H₄)2C₁₃H₆C₁₂H₂₆

Guidance literature:: Multi-step reaction with 3 steps

1.1: Mg; 1,2-dibromoethane

1.2: 72 percent / diethyl ether / 1 h / Heating

2.1: 61 percent / MeSO₃H / CH₂Cl₂ / 0.08 h / 20 °C

3.1: 1.96 g / hexaethylguanidinium chloride; K₂CO₃ / Pd(PPh₃)4 / toluene / 23 h / Heating

With methanesulfonic acid; hexaethylguanidinium chloride; potassium carbonate; magnesium; ethylene dibromide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In dichloromethane; toluene; 3.1: Suzuki coupling;
DOI:10.1021/ma0518353