sodium 2-carboxy-2-(N-acetylamino)-3-(3,5-di-tert-butyl-4-hydroxyphenyl)propanoate

Base Information

• Chemical Name: sodium 2-carboxy-2-(N-acetylamino)-3-(3,5-di-tert-butyl-4-hydroxyphenyl)propanoate
• CAS No.: 1242101-67-2
• Molecular Formula: C₂₀H₂₈NO₆*Na
• Molecular Weight: 401.435

Synonyms:sodium 2-carboxy-2-(N-acetylamino)-3-(3,5-di-tert-butyl-4-hydroxyphenyl)propanoate

Chemical Property of sodium 2-carboxy-2-(N-acetylamino)-3-(3,5-di-tert-butyl-4-hydroxyphenyl)propanoate

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Technology Process of sodium 2-carboxy-2-(N-acetylamino)-3-(3,5-di-tert-butyl-4-hydroxyphenyl)propanoate

There total 3 articles about sodium 2-carboxy-2-(N-acetylamino)-3-(3,5-di-tert-butyl-4-hydroxyphenyl)propanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

diethyl N-acetylamino-(3,5-di-tert-butyl-4-hydroxybenzyl)malonate (67739-21-3) → sodium 2-carboxy-2-(N-acetylamino)-3-(3,5-di-tert-butyl-4-hydroxyphenyl)propanoate (1242101-67-2)

Guidance literature:

With sodium hydroxide; In 1,4-dioxane; water; at 85 - 90 ℃; for 2h; Inert atmosphere;

DOI:10.1007/s11172-009-0115-2

Reference yield: 62.0%

diethyl N-acetylamino-(3,5-di-tert-butyl-4-hydroxybenzyl)malonate (67739-21-3) → sodium 2-carboxy-2-(N-acetylamino)-3-(3,5-di-tert-butyl-4-hydroxyphenyl)propanoate (1242101-67-2) + 2-N-acetylamino-3-(3,5-di-tert-butyl-4-hydroxyphenyl)propanoic acid

Guidance literature:

With sodium hydroxide; In 1,4-dioxane; water; at 85 - 90 ℃; for 2h; Inert atmosphere;

DOI:10.1080/15421406.2012.635512

Reference yield:

diethyl N-acetylamino-(3,5-di-tert-butyl-4-hydroxybenzyl)malonate (67739-21-3) → 2-N-acetylamino(3,5-di-tert-butyl-4-hydroxyphenyl)propanoic acid sodium salt (1242101-71-8) + sodium 2-carboxy-2-(N-acetylamino)-3-(3,5-di-tert-butyl-4-hydroxyphenyl)propanoate (1242101-67-2) + C22H32NO6(1-)*Na(1+) (1242101-68-3)

Guidance literature:

With sodium hydroxide; In 1,4-dioxane; water; at 100 ℃; Inert atmosphere;

DOI:10.1080/15421406.2012.635512

upstream raw materials:

diethyl N-acetylamino-(3,5-di-tert-butyl-4-hydroxybenzyl)malonate

Downstream raw materials:

2-N-acetylamino(3,5-di-tert-butyl-4-hydroxyphenyl)propanoic acid sodium salt

N-acetylamino(3,5-di-tert-butyl-4-hydroxybenzyl)malonic acid

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