IrCl(CO)(P(C₆H₅)3)2(S₂O)

Base Information

Chemical Name:IrCl(CO)(P(C₆H₅)3)2(S₂O)
CAS No.:117256-63-0
Molecular Formula:C₃₇H₃₀ClIrO₂P₂S₂
Molecular Weight:860.397
Hs Code.:

IrCl(CO)(P(C<sub>6</sub>H<sub>5</sub>)3)2(S<sub>2</sub>O)

Synonyms:IrCl(CO)(P(C₆H₅)3)2(S₂O)

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Chemical Property of IrCl(CO)(P(C₆H₅)3)2(S₂O)

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Technology Process of IrCl(CO)(P(C₆H₅)3)2(S₂O)

There total 2 articles about IrCl(CO)(P(C₆H₅)3)2(S₂O) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 117256-61-8
IrCl(CO)(PPh₃)2(OSNSO₂C₆H₄Me-4)

: 15318-31-7,14871-41-1,59246-46-7
bis(triphenylphosphine)iridium(I) carbonyl chloride

: 117256-63-0
IrCl(CO)(P(C₆H₅)3)2(S₂O)

Guidance literature:: With hydrogen sulfide; In tetrahydrofuran; treatment of suspn. of Ir-compd. with H2S (20 s), sealing, stirring (20 min); removal of solvent (vac.), dissoln. (CH2Cl2), chromy. (silica gel, CH2Cl2 and CH2Cl2/THF 10/1), removal of solvent, chromy. (silica gel, CH2Cl2/THF 10/1), recrystn. (THF/EtOH); elem. anal.;
DOI:10.1016/0022-328X(90)87181-C

Reference yield: 76.0%

: 117256-61-8
IrCl(CO)(P(C₆H₅)3)2(CH₃C₆H₄SO₂NSO)

: 59246-46-7,14871-41-1,15318-31-7
bis(triphenylphosphine)carbonyliridium(I) chloride

: 117256-63-0
IrCl(CO)(P(C₆H₅)3)2(S₂O)

Guidance literature:: With hydrogen sulfide; In tetrahydrofuran; N2, H2S-stream, 20 s, stirring for 20 min; evapn., dissolving in minimum of CH2Cl2, chromy. (silica gel, CH2Cl2, then CH2Cl2/THF 10/1), evapn., thin-layer chromy. (silica gel, CH2Cl2/THF 10/1), crystn. from THF/EtOH, elem. anal.;