(4S)-N⁸-(benzyloxycarbonyl)-N⁴-(tert-butoxycarbonyl)-4,8-diamino-2-octene-1-ol

Base Information

Chemical Name:(4S)-N⁸-(benzyloxycarbonyl)-N⁴-(tert-butoxycarbonyl)-4,8-diamino-2-octene-1-ol
CAS No.:124754-93-4
Molecular Formula:C₂₁H₃₂N₂O₅
Molecular Weight:392.495
Hs Code.:

(4S)-N<sup>8</sup>-(benzyloxycarbonyl)-N<sup>4</sup>-(tert-butoxycarbonyl)-4,8-diamino-2-octene-1-ol

Synonyms:(4S)-N⁸-(benzyloxycarbonyl)-N⁴-(tert-butoxycarbonyl)-4,8-diamino-2-octene-1-ol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (4S)-N⁸-(benzyloxycarbonyl)-N⁴-(tert-butoxycarbonyl)-4,8-diamino-2-octene-1-ol

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Technology Process of (4S)-N⁸-(benzyloxycarbonyl)-N⁴-(tert-butoxycarbonyl)-4,8-diamino-2-octene-1-ol

There total 1 articles about (4S)-N⁸-(benzyloxycarbonyl)-N⁴-(tert-butoxycarbonyl)-4,8-diamino-2-octene-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 82689-16-5
benzyl {(5S)-5-[(tert-butoxycarbonyl)amino]-6-oxohexyl}carbamate

: 124754-93-4
(4S)-N⁸-(benzyloxycarbonyl)-N⁴-(tert-butoxycarbonyl)-4,8-diamino-2-octene-1-ol

Guidance literature:: Multi-step reaction with 2 steps

1: 84 percent / benzene / 16 h / Ambient temperature

2: 1.) BF₃*Et₂O, 2.) i-Bu₂AlH / 1.) CH₂Cl₂, -78 deg C, 15 min, 2.) hexane, 1 h

With boron trifluoride diethyl etherate; diisobutylaluminium hydride; In benzene;

Reference yield: 100.0%

: 124754-93-4
(4S)-N⁸-(benzyloxycarbonyl)-N⁴-(tert-butoxycarbonyl)-4,8-diamino-2-octene-1-ol

: 124754-56-9
(4S)-N⁸-(benzyloxycarbonyl)-N⁴-(tert-butoxycarbonyl)-4,8-diamino-1-chloro-2-octene

Guidance literature:: With N-chloro-succinimide; triphenylphosphine; In dichloromethane; at 0 ℃; for 1h;

Reference yield:

: 124754-93-4
(4S)-N⁸-(benzyloxycarbonyl)-N⁴-(tert-butoxycarbonyl)-4,8-diamino-2-octene-1-ol

: 124754-58-1
C₂₃H₃₇ClN₂O₄Si

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / Ph₃P, N-chlorosuccinimide / CH₂Cl₂ / 1 h / 0 °C

2: 2,6-lutidine / CH₂Cl₂ / 0.25 h / Ambient temperature

With 2,6-dimethylpyridine; N-chloro-succinimide; triphenylphosphine; In dichloromethane;