6-amino-1,3-dimethyl-5-(2-nitro-1-phenylethyl)pyrimidine-2,4(1H,3H)-dione

Base Information

Chemical Name:6-amino-1,3-dimethyl-5-(2-nitro-1-phenylethyl)pyrimidine-2,4(1H,3H)-dione
CAS No.:95834-23-4
Molecular Formula:C₁₄H₁₆N₄O₄
Molecular Weight:304.305
Hs Code.:

Synonyms:6-amino-1,3-dimethyl-5-(2-nitro-1-phenylethyl)pyrimidine-2,4(1H,3H)-dione

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 6-amino-1,3-dimethyl-5-(2-nitro-1-phenylethyl)pyrimidine-2,4(1H,3H)-dione

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Technology Process of 6-amino-1,3-dimethyl-5-(2-nitro-1-phenylethyl)pyrimidine-2,4(1H,3H)-dione

There total 2 articles about 6-amino-1,3-dimethyl-5-(2-nitro-1-phenylethyl)pyrimidine-2,4(1H,3H)-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 5153-67-3
nitrostyrene

: 104497-09-8
6-amino-1,3-dimethylbarbituric acid

: 95834-23-4
6-amino-1,3-dimethyl-5-(2-nitro-1-phenylethyl)pyrimidine-2,4(1H,3H)-dione

Guidance literature:: With 2Zn⁽²⁺⁾*2NO₃^(1-)*2C₃H₇NO*2Y⁽³⁺⁾*4C₁₄H₁₁NO₃^(2-); In ethanol; water; at 20 ℃; for 0.25h;
DOI:10.1021/acs.inorgchem.7b01011

Reference yield: 95.0%

: 5153-67-3
nitrostyrene

: 6642-31-5
6-Amino-1,3-dimethylbarbituric acid

: 95834-23-4
6-amino-1,3-dimethyl-5-(2-nitro-1-phenylethyl)pyrimidine-2,4(1H,3H)-dione

Guidance literature:: With sodium hydroxide; In ethanol; water; at 20 ℃; for 1h;
DOI:10.1016/j.bmcl.2015.12.047

Reference yield: 92.0%

: 95834-23-4
6-amino-1,3-dimethyl-5-(2-nitro-1-phenylethyl)pyrimidine-2,4(1H,3H)-dione

: 36896-69-2
1,3-dimethyl-5-phenyl-1H-pyrrolo[2,3-d]pyrimidine-2,4(3H,7H)-dione

Guidance literature:: With sodium dithionite; sodium hydroxide; In water; at 60 ℃; for 1h; Solvent; Temperature; Time;
DOI:10.1016/j.bmcl.2015.12.047