C₃₅H₄₅IO₁₀Si

Base Information

Chemical Name:C₃₅H₄₅IO₁₀Si
CAS No.:923976-66-3
Molecular Formula:C₃₅H₄₅IO₁₀Si
Molecular Weight:780.726
Hs Code.:

C<sub>35</sub>H<sub>45</sub>IO<sub>10</sub>Si

Synonyms:C₃₅H₄₅IO₁₀Si

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Chemical Property of C₃₅H₄₅IO₁₀Si

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Technology Process of C₃₅H₄₅IO₁₀Si

There total 9 articles about C₃₅H₄₅IO₁₀Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: C₃₉H₅₅N₃O₁₀Si

: 923976-66-3
C₃₅H₄₅IO₁₀Si

Guidance literature:: With iodine; methyl iodide; at 110 ℃; for 336000h;
DOI:10.1021/ja053530+

Reference yield:

: 3,3-diethyl-1-(2-iodo-4-benzoic acid)-1-triazene

: 923976-66-3
C₃₅H₄₅IO₁₀Si

Guidance literature:: Multi-step reaction with 5 steps

1.1: dimethylaminopyridine; 1-ethyl-3-(3-dimethylaminopropyl)carbodiimide / CH₂Cl₂ / 0.33 h / 0 °C

1.2: 91 percent / CH₂Cl₂ / 0 - 20 °C

2.1: 99 percent / Pd(PPh₃)2Cl₂; CuI; Et₃N / 20 °C

3.1: 86 percent / I₂; MeI / 1 h / 150 °C / microwave irradiation

4.1: 81 percent / Pd(PPh₃)2Cl₂; CuI; Et₃N / tetrahydrofuran / 55 °C

5.1: 75 percent / MeI; I₂ / 336000 h / 110 °C

With dmap; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; iodine; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; triethylamine; methyl iodide; In tetrahydrofuran; dichloromethane; 2.1: Sonogashira coupling / 4.1: Sonogashira coupling;
DOI:10.1021/ja053530+

Reference yield:

: 3,3-diethyl-1-{2-iodo-4-benzoic acid 2-[2-(2-methoxy-ethoxy)-ethoxy]-ethyl ester}-1-triazene

: 923976-66-3
C₃₅H₄₅IO₁₀Si

Guidance literature:: Multi-step reaction with 4 steps

1: 99 percent / Pd(PPh₃)2Cl₂; CuI; Et₃N / 20 °C

2: 86 percent / I₂; MeI / 1 h / 150 °C / microwave irradiation

3: 81 percent / Pd(PPh₃)2Cl₂; CuI; Et₃N / tetrahydrofuran / 55 °C

4: 75 percent / MeI; I₂ / 336000 h / 110 °C

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; iodine; triethylamine; methyl iodide; In tetrahydrofuran; 1: Sonogashira coupling / 3: Sonogashira coupling;
DOI:10.1021/ja053530+