N¹-phenyl-N⁴[4-(1-oxyl-4,5-dihydro-1H-imidazol-2-yl)-2,6-dinitrophenyl]-1,4-benzenediimine N¹[4-(1-oxyl-4,5-dihydro-1H-imidazol-2-yl)-2,6-dinitrophenyl]imine diradical

Base Information

• Chemical Name: N¹-phenyl-N⁴[4-(1-oxyl-4,5-dihydro-1H-imidazol-2-yl)-2,6-dinitrophenyl]-1,4-benzenediimine N¹[4-(1-oxyl-4,5-dihydro-1H-imidazol-2-yl)-2,6-dinitrophenyl]imine diradical
• CAS No.: 1478732-78-3
• Molecular Formula: C₃₈H₃₇N₁₁O₁₀
• Molecular Weight: 807.779

Synonyms:N¹-phenyl-N⁴[4-(1-oxyl-4,5-dihydro-1H-imidazol-2-yl)-2,6-dinitrophenyl]-1,4-benzenediimine N¹[4-(1-oxyl-4,5-dihydro-1H-imidazol-2-yl)-2,6-dinitrophenyl]imine diradical

Chemical Property of N¹-phenyl-N⁴[4-(1-oxyl-4,5-dihydro-1H-imidazol-2-yl)-2,6-dinitrophenyl]-1,4-benzenediimine N¹[4-(1-oxyl-4,5-dihydro-1H-imidazol-2-yl)-2,6-dinitrophenyl]imine diradical

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Technology Process of N¹-phenyl-N⁴[4-(1-oxyl-4,5-dihydro-1H-imidazol-2-yl)-2,6-dinitrophenyl]-1,4-benzenediimine N¹[4-(1-oxyl-4,5-dihydro-1H-imidazol-2-yl)-2,6-dinitrophenyl]imine diradical

There total 7 articles about N¹-phenyl-N⁴[4-(1-oxyl-4,5-dihydro-1H-imidazol-2-yl)-2,6-dinitrophenyl]-1,4-benzenediimine N¹[4-(1-oxyl-4,5-dihydro-1H-imidazol-2-yl)-2,6-dinitrophenyl]imine diradical which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 25.0%

C38H45N11O12 → N1-phenyl-N4[4-(1-oxyl-4,5-dihydro-1H-imidazol-2-yl)-2,6-dinitrophenyl]-1,4-benzenediimine N1[4-(1-oxyl-4,5-dihydro-1H-imidazol-2-yl)-2,6-dinitrophenyl]imine diradical (1478732-78-3)

Guidance literature:

With lead dioxide; sodium sulfate; In dichloromethane; for 1h;

DOI:10.3998/ark.5550190.p008.314

Reference yield:

4-chloro-3,5-dinitrobenzonitrile (1930-72-9) → N1-phenyl-N4[4-(1-oxyl-4,5-dihydro-1H-imidazol-2-yl)-2,6-dinitrophenyl]-1,4-benzenediimine N1[4-(1-oxyl-4,5-dihydro-1H-imidazol-2-yl)-2,6-dinitrophenyl]imine diradical (1478732-78-3)

Guidance literature:

Multi-step reaction with 6 steps

1: sodium hydrogencarbonate / ethanol / 2 h / Reflux

2: sodium sulfate; lead dioxide / dichloromethane / 6 h

3: ascorbic acid / dichloromethane; water

4: diisobutylaluminium hydride / dichloromethane / 1 h / -78 - 20 °C / Cooling with acetone-dry ice

5: dichloromethane / 72 h

6: sodium sulfate; lead dioxide / dichloromethane / 1 h

With diisobutylaluminium hydride; sodium hydrogencarbonate; lead dioxide; sodium sulfate; ascorbic acid; In ethanol; dichloromethane; water;

DOI:10.3998/ark.5550190.p008.314

Reference yield:

N,N-diphenylhydrazine hydrochloride (530-47-2,29666-92-0) → N1-phenyl-N4[4-(1-oxyl-4,5-dihydro-1H-imidazol-2-yl)-2,6-dinitrophenyl]-1,4-benzenediimine N1[4-(1-oxyl-4,5-dihydro-1H-imidazol-2-yl)-2,6-dinitrophenyl]imine diradical (1478732-78-3)

Guidance literature:

Multi-step reaction with 6 steps

1: sodium hydrogencarbonate / ethanol / 2 h / Reflux

2: sodium sulfate; lead dioxide / dichloromethane / 6 h

3: ascorbic acid / dichloromethane; water

4: diisobutylaluminium hydride / dichloromethane / 1 h / -78 - 20 °C / Cooling with acetone-dry ice

5: dichloromethane / 72 h

6: sodium sulfate; lead dioxide / dichloromethane / 1 h

With diisobutylaluminium hydride; sodium hydrogencarbonate; lead dioxide; sodium sulfate; ascorbic acid; In ethanol; dichloromethane; water;

DOI:10.3998/ark.5550190.p008.314

upstream raw materials:

4-chloro-3,5-dinitrobenzonitrile

N,N-diphenylhydrazine hydrochloride

4-(N',N'-diphenylhydrazin-yl)-3,5-dinitrobenzonitrile

4-(methoxyamino)-3,5-dinitrobenzonitrile

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