{Pd₂CoCl(CO)3(dppm)2}

Base Information

Chemical Name:{Pd₂CoCl(CO)3(dppm)2}
CAS No.:113109-26-5
Molecular Formula:C₅₃H₄₄ClCoO₃P₄Pd₂
Molecular Weight:1160.11
Hs Code.:

Synonyms:{Pd₂CoCl(CO)3(dppm)2}

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Chemical Property of {Pd₂CoCl(CO)3(dppm)2}

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Technology Process of {Pd₂CoCl(CO)3(dppm)2}

There total 5 articles about {Pd₂CoCl(CO)3(dppm)2} which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: tetrafluoroboric acid

: 113109-24-3
{Pd₂Co₂(CO)7(dppm)2}

: 113109-26-5
{Pd₂CoCl(CO)3(dppm)2}

Guidance literature:: With sodium chloride; In tetrahydrofuran; water; This synthesis was performed by adding NaCl in water and aq. HBF4 to an acetone soln. of Pd2Co2(CO)7(dppm)2.; The soln. was filtered to remove some insol. CoCl2. n-Hexane was added to the soln., and the resulting solid was collected by filtration, washed with water, and dried in vac. Recrystn. in CH2Cl2/n-hexane.;

Reference yield: 80.0%

: 113109-24-3
{Pd₂Co₂(CO)7(dppm)2}

: 113109-26-5
{Pd₂CoCl(CO)3(dppm)2}

Guidance literature:: With NaCl; In water; acetone; byproducts: Na{Co(CO)4}; A soln. of NaCl in a mixt. of acetone and H2O was added to a soln. of {Pd2Co2(CO)7(dppm)2} in acetone.; n-C6H14 was added, and stirring led {Pd2CoCl(CO)3(dppm)2} to ppt. in the org. phase. It was collected by filtration and dried. Dissolution in toluene and filtration afforded a soln., which after addn. of n-C6H14 gave a powder. Elem.anal.;

Reference yield: 58.0%

: 113109-24-3
{Pd₂Co₂(CO)7(dppm)2}

: 38425-01-3
(bis(diphenylphosphino)methane)palladium(II) dichloride

: 113109-26-5
{Pd₂CoCl(CO)3(dppm)2}

Guidance literature:: With hydrogenchloride; In tetrahydrofuran; water; byproducts: cobalt chloride; HCl n(37% in water) was added to a THF soln. of Pd2Co2(CO)7(dppm)2, which was then stirred overnight.; The soln. was filtered to remove some insol. CoCl2. n-C6H14 was added to the soln., and the resulting solid was collected by filtration, washed with H2O, and dried in vac. Recrystn. in CH2Cl2/n-hexane. Contaminated with {PdCl2(μ-dppm)}.;