adamantane-2-spiro-3'-5',5'-bis[4'-(ethoxycarbonyl)phenyl]-1',2',4'-trioxolane

Base Information

Chemical Name:adamantane-2-spiro-3'-5',5'-bis[4'-(ethoxycarbonyl)phenyl]-1',2',4'-trioxolane
CAS No.:664336-96-3
Molecular Formula:C₂₉H₃₂O₇
Molecular Weight:492.569
Hs Code.:

Synonyms:adamantane-2-spiro-3'-5',5'-bis[4'-(ethoxycarbonyl)phenyl]-1',2',4'-trioxolane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of adamantane-2-spiro-3'-5',5'-bis[4'-(ethoxycarbonyl)phenyl]-1',2',4'-trioxolane

Chemical Property:

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Technology Process of adamantane-2-spiro-3'-5',5'-bis[4'-(ethoxycarbonyl)phenyl]-1',2',4'-trioxolane

There total 3 articles about adamantane-2-spiro-3'-5',5'-bis[4'-(ethoxycarbonyl)phenyl]-1',2',4'-trioxolane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 36.0%

: 76300-15-7
adamantan-2-one O-methyloxime

: 1797-82-6
diethyl 4,4'-benzophenonedicarboxylate

: 664336-96-3
adamantane-2-spiro-3'-5',5'-bis[4'-(ethoxycarbonyl)phenyl]-1',2',4'-trioxolane

Guidance literature:: With ozone; In dichloromethane; pentane; at 0 ℃;
DOI:10.1016/j.bmc.2006.05.041

Reference yield:

: 611-97-2
bis(p-methylphenyl)-methanone

: 664336-96-3
adamantane-2-spiro-3'-5',5'-bis[4'-(ethoxycarbonyl)phenyl]-1',2',4'-trioxolane

Guidance literature:: Multi-step reaction with 3 steps

1: 80 percent / KMnO₄

2: 90 percent / H₂SO₄ / toluene / Heating

3: 36 percent / ozone / pentane; CH₂Cl₂ / 0 °C

With potassium permanganate; sulfuric acid; ozone; In dichloromethane; toluene; pentane;
DOI:10.1016/j.bmc.2006.05.041

Reference yield:

: 964-68-1
4,4'-benzophenonedicarboxylic acid

: 664336-96-3
adamantane-2-spiro-3'-5',5'-bis[4'-(ethoxycarbonyl)phenyl]-1',2',4'-trioxolane

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / H₂SO₄ / toluene / Heating

2: 36 percent / ozone / pentane; CH₂Cl₂ / 0 °C

With sulfuric acid; ozone; In dichloromethane; toluene; pentane;
DOI:10.1016/j.bmc.2006.05.041