1-[3-(t-butyl-diphenyl-silanyloxy)-1-methylene-propyl]-2-isopropenyl-5,5-dimethylcyclohexanol

Base Information

Chemical Name:1-[3-(t-butyl-diphenyl-silanyloxy)-1-methylene-propyl]-2-isopropenyl-5,5-dimethylcyclohexanol
CAS No.:848122-36-1
Molecular Formula:C₃₁H₄₄O₂Si
Molecular Weight:476.775
Hs Code.:

Synonyms:1-[3-(t-butyl-diphenyl-silanyloxy)-1-methylene-propyl]-2-isopropenyl-5,5-dimethylcyclohexanol

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Chemical Property of 1-[3-(t-butyl-diphenyl-silanyloxy)-1-methylene-propyl]-2-isopropenyl-5,5-dimethylcyclohexanol

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Technology Process of 1-[3-(t-butyl-diphenyl-silanyloxy)-1-methylene-propyl]-2-isopropenyl-5,5-dimethylcyclohexanol

There total 2 articles about 1-[3-(t-butyl-diphenyl-silanyloxy)-1-methylene-propyl]-2-isopropenyl-5,5-dimethylcyclohexanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 848122-40-7
tert-butyl((3-iodobut-3-en-1-yl)oxy)diphenylsilane

: 848122-34-9
2-isopropenyl-5,5-dimethyl-cyclohexanone

: 848122-36-1
1-[3-(t-butyl-diphenyl-silanyloxy)-1-methylene-propyl]-2-isopropenyl-5,5-dimethylcyclohexanol

Guidance literature:: tert-butyl((3-iodobut-3-en-1-yl)oxy)diphenylsilane; With tert.-butyl lithium; In diethyl ether; at -90 ℃; for 0.166667h;

2-isopropenyl-5,5-dimethyl-cyclohexanone; In diethyl ether; at -90 ℃;
DOI:10.1021/jo047916z

Reference yield:

: 16750-82-6
(S)-isopiperitenone

: 848122-36-1
1-[3-(t-butyl-diphenyl-silanyloxy)-1-methylene-propyl]-2-isopropenyl-5,5-dimethylcyclohexanol

Guidance literature:: Multi-step reaction with 2 steps

1.1: CuI / diethyl ether / -10 °C

1.2: 83 percent / diethyl ether / -10 - 20 °C

2.1: t-BuLi / diethyl ether / 0.17 h / -90 °C

2.2: 87 percent / diethyl ether / -90 °C

With copper(l) iodide; tert.-butyl lithium; In diethyl ether;
DOI:10.1021/jo047916z