N-(1-methyl-1H-pyrazol-3-yl)-3-[(phenylmethyl)oxy]-5-[(3S)-tetrahydrofuran-3-yloxy]benzamide

Base Information

Chemical Name:N-(1-methyl-1H-pyrazol-3-yl)-3-[(phenylmethyl)oxy]-5-[(3S)-tetrahydrofuran-3-yloxy]benzamide
CAS No.:915771-03-8
Molecular Formula:C₂₂H₂₃N₃O₄
Molecular Weight:393.442
Hs Code.:

Synonyms:N-(1-methyl-1H-pyrazol-3-yl)-3-[(phenylmethyl)oxy]-5-[(3S)-tetrahydrofuran-3-yloxy]benzamide

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Chemical Property of N-(1-methyl-1H-pyrazol-3-yl)-3-[(phenylmethyl)oxy]-5-[(3S)-tetrahydrofuran-3-yloxy]benzamide

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Technology Process of N-(1-methyl-1H-pyrazol-3-yl)-3-[(phenylmethyl)oxy]-5-[(3S)-tetrahydrofuran-3-yloxy]benzamide

There total 4 articles about N-(1-methyl-1H-pyrazol-3-yl)-3-[(phenylmethyl)oxy]-5-[(3S)-tetrahydrofuran-3-yloxy]benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 915771-04-9
3-hydroxy-N-(1-methyl-1H-pyrazol-3-yl)-5-[(phenylmethyl)oxy]benzamide

: 219823-47-9
(R)-tetrahydrofuran-3-yl 4-methylbenzenesulfonate

: 915771-03-8
N-(1-methyl-1H-pyrazol-3-yl)-3-[(phenylmethyl)oxy]-5-[(3S)-tetrahydrofuran-3-yloxy]benzamide

Guidance literature:: With potassium carbonate; In acetonitrile; at 160 ℃; for 3h; Microwave irradiation;

Reference yield:

: 915771-05-0
N-(1-methyl-1H-pyrazol-3-yl)-3,5-bis[(phenylmethyl)oxy]benzamide

: 915771-03-8
N-(1-methyl-1H-pyrazol-3-yl)-3-[(phenylmethyl)oxy]-5-[(3S)-tetrahydrofuran-3-yloxy]benzamide

Guidance literature:: Multi-step reaction with 2 steps

1: ammonium formate / palladium 10% on activated carbon / ethanol / 0.08 h / 140 °C / Microwave

2: potassium carbonate / acetonitrile / 3 h / 160 °C / Microwave

With ammonium formate; potassium carbonate; palladium 10% on activated carbon; In ethanol; acetonitrile;

Reference yield:

: 28917-43-3
3,5-dibenzyloxybenzoic acid

: 915771-03-8
N-(1-methyl-1H-pyrazol-3-yl)-3-[(phenylmethyl)oxy]-5-[(3S)-tetrahydrofuran-3-yloxy]benzamide

Guidance literature:: Multi-step reaction with 4 steps

1: oxalyl dichloride / dichloromethane / 6 h / 20 °C

2: dichloromethane / 16 h / 20 °C

3: ammonium formate / palladium 10% on activated carbon / ethanol / 0.08 h / 140 °C / Microwave

4: potassium carbonate / acetonitrile / 3 h / 160 °C / Microwave

With oxalyl dichloride; ammonium formate; potassium carbonate; palladium 10% on activated carbon; In ethanol; dichloromethane; acetonitrile;