Dithiophosphoric acid S-[1,3-bis-(4-chloro-phenyl)-3-oxo-propyl] ester O,O'-diethyl ester

Base Information

• Chemical Name: Dithiophosphoric acid S-[1,3-bis-(4-chloro-phenyl)-3-oxo-propyl] ester O,O'-diethyl ester
• CAS No.: 79359-73-2
• Molecular Formula: C₁₉H₂₁Cl₂O₃PS₂
• Molecular Weight: 463.386

Synonyms:Dithiophosphoric acid S-[1,3-bis-(4-chloro-phenyl)-3-oxo-propyl] ester O,O'-diethyl ester

Chemical Property of Dithiophosphoric acid S-[1,3-bis-(4-chloro-phenyl)-3-oxo-propyl] ester O,O'-diethyl ester

Chemical Property:

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Technology Process of Dithiophosphoric acid S-[1,3-bis-(4-chloro-phenyl)-3-oxo-propyl] ester O,O'-diethyl ester

There total 1 articles about Dithiophosphoric acid S-[1,3-bis-(4-chloro-phenyl)-3-oxo-propyl] ester O,O'-diethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

1,3-bis(4-chlorophenyl)prop-2-en-1-one (20725-25-1,22966-30-9,19672-59-4) + O,O-Diethyl hydrogen phosphorodithioate (298-06-6) → Dithiophosphoric acid S-[1,3-bis-(4-chloro-phenyl)-3-oxo-propyl] ester O,O'-diethyl ester (79359-73-2)

Guidance literature:

In benzene; at 50 - 60 ℃; for 3h;

DOI:10.1055/s-1981-29521

Reference yield: 92.0%

sodium cyanide (143-33-9,25596-52-5) + Dithiophosphoric acid S-[1,3-bis-(4-chloro-phenyl)-3-oxo-propyl] ester O,O'-diethyl ester (79359-73-2) → (2S,4S)-2,4-Bis-(4-chloro-phenyl)-thietane-2-carbonitrile

Guidance literature:

for 0.0333333h; microwave irradiation;

DOI:10.1055/s-2002-33337

Reference yield: 88.0%

Dithiophosphoric acid S-[1,3-bis-(4-chloro-phenyl)-3-oxo-propyl] ester O,O'-diethyl ester (79359-73-2) + sodium thiomethoxide (5188-07-8) → (2S,4S)-2,4-Bis-(4-chloro-phenyl)-2-methylsulfanyl-thietane

Guidance literature:

for 0.0416667h; microwave irradiation;

DOI:10.1055/s-2002-33337

upstream raw materials:

1,3-bis(4-chlorophenyl)prop-2-en-1-one

O,O-Diethyl hydrogen phosphorodithioate

Downstream raw materials:

2,4-bis(4-chlorophenyl)thietane

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