C₅₅H₅₁N₅O₆SSi

Base Information

Chemical Name:C₅₅H₅₁N₅O₆SSi
CAS No.:1092803-52-5
Molecular Formula:C₅₅H₅₁N₅O₆SSi
Molecular Weight:938.191
Hs Code.:

C<sub>55</sub>H<sub>51</sub>N<sub>5</sub>O<sub>6</sub>SSi

Synonyms:C₅₅H₅₁N₅O₆SSi

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₅₅H₅₁N₅O₆SSi

Chemical Property:

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Technology Process of C₅₅H₅₁N₅O₆SSi

There total 12 articles about C₅₅H₅₁N₅O₆SSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 956485-06-6
3-O-(2-naphthylmethyl)-1,2:5,6-di-O-isopropylidene-α-D-allofuranose

: 1092803-52-5
C₅₅H₅₁N₅O₆SSi

Guidance literature:: Multi-step reaction with 14 steps

1.1: water; acetic acid / 16 h / 20 °C

2.1: sodium periodate / 1,4-dioxane; water / 1.67 h

3.1: sodium hydroxide / water; tetrahydrofuran / 72 h / 20 °C / Cooling with ice

4.1: triethylamine / dichloromethane; methanol / 18 h / 0 - 20 °C

5.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.75 h / -78 °C

6.1: n-butyllithium / tetrahydrofuran / 2 h / 0 °C

6.2: 16.33 h / -78 - 20 °C

7.1: 9-bora-bicyclo[3.3.1]nonane / tetrahydrofuran / 24 h / 20 °C

7.2: 4 h / 50 °C

8.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.75 h / -78 °C

8.2: 0.5 h

9.1: triphenylphosphine / dichloromethane / 0.5 h / 0 °C

9.2: 2 h / -78 °C

10.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone; water / dichloromethane / 6 h / 20 °C

11.1: tetrahydrofuran; hexanes / 0.5 h / -78 °C

12.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 4 h / 0 - 20 °C

13.1: acetic anhydride; sulfuric acid; acetic acid

13.2: Reflux

14.1: dmap

With dmap; sodium periodate; n-butyllithium; oxalyl dichloride; sulfuric acid; water; acetic anhydride; sodium hydride; acetic acid; dimethyl sulfoxide; triethylamine; 9-bora-bicyclo[3.3.1]nonane; triphenylphosphine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; sodium hydroxide; In tetrahydrofuran; 1,4-dioxane; methanol; hexanes; dichloromethane; water; N,N-dimethyl-formamide; mineral oil; 13.2: Vorbrugen Reaction;

Reference yield:

: 1091607-89-4
(R)-1-((3aR,5R,6R,6aR)-2,2-dimethyl-6-(naphthalen-2-ylmethoxy)tetrahydrofuro[3,2-d][1,3]dioxol-5-yl)ethane-1,2-diol

: 1092803-52-5
C₅₅H₅₁N₅O₆SSi

Guidance literature:: Multi-step reaction with 13 steps

1.1: sodium periodate / 1,4-dioxane; water / 1.67 h

2.1: sodium hydroxide / water; tetrahydrofuran / 72 h / 20 °C / Cooling with ice

3.1: triethylamine / dichloromethane; methanol / 18 h / 0 - 20 °C

4.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.75 h / -78 °C

5.1: n-butyllithium / tetrahydrofuran / 2 h / 0 °C

5.2: 16.33 h / -78 - 20 °C

6.1: 9-bora-bicyclo[3.3.1]nonane / tetrahydrofuran / 24 h / 20 °C

6.2: 4 h / 50 °C

7.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.75 h / -78 °C

7.2: 0.5 h

8.1: triphenylphosphine / dichloromethane / 0.5 h / 0 °C

8.2: 2 h / -78 °C

9.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone; water / dichloromethane / 6 h / 20 °C

10.1: tetrahydrofuran; hexanes / 0.5 h / -78 °C

11.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 4 h / 0 - 20 °C

12.1: acetic anhydride; sulfuric acid; acetic acid

12.2: Reflux

13.1: dmap

With dmap; sodium periodate; n-butyllithium; oxalyl dichloride; sulfuric acid; water; acetic anhydride; sodium hydride; acetic acid; dimethyl sulfoxide; triethylamine; 9-bora-bicyclo[3.3.1]nonane; triphenylphosphine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; sodium hydroxide; In tetrahydrofuran; 1,4-dioxane; methanol; hexanes; dichloromethane; water; N,N-dimethyl-formamide; mineral oil; 12.2: Vorbrugen Reaction;

Reference yield:

: 1057385-93-9
(3aR,5S,6R,6aR)-2,2-dimethyl-6-(naphthalen-2-ylmethoxy)tetrahydrofuro[3,2-d][1,3]dioxole-5-carbaldehyde

: 1092803-52-5
C₅₅H₅₁N₅O₆SSi

Guidance literature:: Multi-step reaction with 12 steps

1.1: sodium hydroxide / water; tetrahydrofuran / 72 h / 20 °C / Cooling with ice

2.1: triethylamine / dichloromethane; methanol / 18 h / 0 - 20 °C

3.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.75 h / -78 °C

4.1: n-butyllithium / tetrahydrofuran / 2 h / 0 °C

4.2: 16.33 h / -78 - 20 °C

5.1: 9-bora-bicyclo[3.3.1]nonane / tetrahydrofuran / 24 h / 20 °C

5.2: 4 h / 50 °C

6.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.75 h / -78 °C

6.2: 0.5 h

7.1: triphenylphosphine / dichloromethane / 0.5 h / 0 °C

7.2: 2 h / -78 °C

8.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone; water / dichloromethane / 6 h / 20 °C

9.1: tetrahydrofuran; hexanes / 0.5 h / -78 °C

10.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 4 h / 0 - 20 °C

11.1: acetic anhydride; sulfuric acid; acetic acid

11.2: Reflux

12.1: dmap

With dmap; n-butyllithium; oxalyl dichloride; sulfuric acid; water; acetic anhydride; sodium hydride; acetic acid; dimethyl sulfoxide; triethylamine; 9-bora-bicyclo[3.3.1]nonane; triphenylphosphine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; sodium hydroxide; In tetrahydrofuran; methanol; hexanes; dichloromethane; water; N,N-dimethyl-formamide; mineral oil; 11.2: Vorbrugen Reaction;