(+)-(1S)-(1α,2α,3β,4α,5β,6β)-3-Ammonio-6-(methylammonio)-1,2,4,5-cyclohexanetetrol Sulfate

Base Information

Chemical Name:(+)-(1S)-(1α,2α,3β,4α,5β,6β)-3-Ammonio-6-(methylammonio)-1,2,4,5-cyclohexanetetrol Sulfate
CAS No.:104712-79-0
Molecular Formula:C₇H₁₆N₂O₄*H₂O₄S
Molecular Weight:290.295
Hs Code.:

Synonyms:(+)-(1S)-(1α,2α,3β,4α,5β,6β)-3-Ammonio-6-(methylammonio)-1,2,4,5-cyclohexanetetrol Sulfate

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Chemical Property of (+)-(1S)-(1α,2α,3β,4α,5β,6β)-3-Ammonio-6-(methylammonio)-1,2,4,5-cyclohexanetetrol Sulfate

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Technology Process of (+)-(1S)-(1α,2α,3β,4α,5β,6β)-3-Ammonio-6-(methylammonio)-1,2,4,5-cyclohexanetetrol Sulfate

There total 3 articles about (+)-(1S)-(1α,2α,3β,4α,5β,6β)-3-Ammonio-6-(methylammonio)-1,2,4,5-cyclohexanetetrol Sulfate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 104713-74-8
(+)-(1S)-Bis<(1α,2α,3β,4α,5β,6β)-3-ammonio-5-O,6-N-carbonyl-6-(methylamino)-1,2,4,5-cyclohexanetetrol> Sulfate

: 104712-79-0
(+)-(1S)-(1α,2α,3β,4α,5β,6β)-3-Ammonio-6-(methylammonio)-1,2,4,5-cyclohexanetetrol Sulfate

Guidance literature:: With barium dihydroxide; sulfuric acid; In water; for 2h; Heating;
DOI:10.1002/jlac.198619861201

Reference yield:

: 104713-72-6
Methyl-carbamic acid (3aS,4S,5R,6S,7S,7aS)-4,7-dihydroxy-3-methyl-2-oxo-6-((R)-1-phenyl-ethylamino)-octahydro-benzooxazol-5-yl ester

: 104712-79-0
(+)-(1S)-(1α,2α,3β,4α,5β,6β)-3-Ammonio-6-(methylammonio)-1,2,4,5-cyclohexanetetrol Sulfate

Guidance literature:: Multi-step reaction with 3 steps

1: 98 percent / p-TsOH / dimethylformamide / 2 h / 80 °C

2: 94 percent / H₂, H₂SO₄ / Pd/C (10percent) / methanol / 24 h / 20 °C / 735.5 Torr

3: 96 percent / Ba(OH)2, H₂SO₄ / H₂O / 2 h / Heating

With barium dihydroxide; sulfuric acid; hydrogen; toluene-4-sulfonic acid; palladium on activated charcoal; In methanol; water; N,N-dimethyl-formamide;
DOI:10.1002/jlac.198619861201

Reference yield:

: 88643-00-9
(-)-(1S)-(1α,2α,3β,4α,5β,6β)-5-O,6-N-Carbonyl-1,2-O-isopropylidene-6-(methylamino)-3-<(R)-(1-phenylethyl)amino>-1,2,4,5-cyclohexanetetrol

: 104712-79-0
(+)-(1S)-(1α,2α,3β,4α,5β,6β)-3-Ammonio-6-(methylammonio)-1,2,4,5-cyclohexanetetrol Sulfate

Guidance literature:: Multi-step reaction with 2 steps

1: 94 percent / H₂, H₂SO₄ / Pd/C (10percent) / methanol / 24 h / 20 °C / 735.5 Torr

2: 96 percent / Ba(OH)2, H₂SO₄ / H₂O / 2 h / Heating

With barium dihydroxide; sulfuric acid; hydrogen; palladium on activated charcoal; In methanol; water;
DOI:10.1002/jlac.198619861201