(S)-2-((1R,2R)-2'-(4-bromophenyl)cyclopropyl)-3-methyl-N,N-diphenylbutanamide

Base Information

Chemical Name:(S)-2-((1R,2R)-2'-(4-bromophenyl)cyclopropyl)-3-methyl-N,N-diphenylbutanamide
CAS No.:1166199-07-0
Molecular Formula:C₂₆H₂₆BrNO
Molecular Weight:448.403
Hs Code.:

Synonyms:(S)-2-((1R,2R)-2'-(4-bromophenyl)cyclopropyl)-3-methyl-N,N-diphenylbutanamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-2-((1R,2R)-2'-(4-bromophenyl)cyclopropyl)-3-methyl-N,N-diphenylbutanamide

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Technology Process of (S)-2-((1R,2R)-2'-(4-bromophenyl)cyclopropyl)-3-methyl-N,N-diphenylbutanamide

There total 2 articles about (S)-2-((1R,2R)-2'-(4-bromophenyl)cyclopropyl)-3-methyl-N,N-diphenylbutanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 952686-36-1
p-bromophenylpropene methyl carbonate

: 857804-29-6
N,N-diphenyl-isovaleramide

: 1166199-07-0
(S)-2-((1R,2R)-2'-(4-bromophenyl)cyclopropyl)-3-methyl-N,N-diphenylbutanamide

: 2-(2'-(4-bromophenyl)cyclopropyl)-3-methyl-N,N-diphenylbutanamide

Guidance literature:: N,N-diphenyl-isovaleramide; With lithium chloride; lithium hexamethyldisilazane; In tetrahydrofuran; at 0 ℃; for 0.333333h; Inert atmosphere;

methyl p-bromophenylallyl carbonate; With bis(η3-allyl-μ-chloropalladium(II)); C₃₇H₃₆FeN₂O₃P; In tetrahydrofuran; at 20 ℃; Inert atmosphere;

With ruthenium trichloride; sodium periodate; N-benzyl-N,N,N-triethylammonium chloride; In water; ethyl acetate; at 20 ℃; optical yield given as %ee; enantioselective reaction; Inert atmosphere;
DOI:10.1021/ja902410w

Reference yield:

: 952686-36-1
p-bromophenylpropene methyl carbonate

: 857804-29-6
N,N-diphenyl-isovaleramide

: C₂₆H₂₆BrNO

: C₂₆H₂₆BrNO

: 1166199-07-0
(S)-2-((1R,2R)-2'-(4-bromophenyl)cyclopropyl)-3-methyl-N,N-diphenylbutanamide

: 2-(2'-(4-bromophenyl)cyclopropyl)-3-methyl-N,N-diphenylbutanamide

Guidance literature:: N,N-diphenyl-isovaleramide; With lithium chloride; lithium hexamethyldisilazane; In tetrahydrofuran; at 0 ℃; for 0.333333h; Inert atmosphere;

methyl p-bromophenylallyl carbonate; With bis(η3-allyl-μ-chloropalladium(II)); C₃₇H₃₆FeN₂O₃P; In tetrahydrofuran; at 20 ℃; optical yield given as %ee; enantioselective reaction; Inert atmosphere;
DOI:10.1021/ja902410w