C₃₇H₄₆N₅O₁₅P

Base Information

Chemical Name:C₃₇H₄₆N₅O₁₅P
CAS No.:1608113-79-6
Molecular Formula:C₃₇H₄₆N₅O₁₅P
Molecular Weight:831.77
Hs Code.:

C<sub>37</sub>H<sub>46</sub>N<sub>5</sub>O<sub>15</sub>P

Synonyms:C₃₇H₄₆N₅O₁₅P

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Chemical Property of C₃₇H₄₆N₅O₁₅P

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Technology Process of C₃₇H₄₆N₅O₁₅P

There total 12 articles about C₃₇H₄₆N₅O₁₅P which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 1608113-78-5
C₂₃H₃₃N₅O₁₂

: 108549-23-1
Dibenzyl N,N-diisopropylphosphoramidite

: 1608113-79-6
C₃₇H₄₆N₅O₁₅P

Guidance literature:: C₂₃H₃₃N₅O₁₂; Dibenzyl N,N-diisopropylphosphoramidite; With 1H-tetrazole; In dichloromethane; acetonitrile; at 0 - 20 ℃; for 12h; Inert atmosphere;

With dihydrogen peroxide; In dichloromethane; acetonitrile; at -40 - 20 ℃; for 2h; Inert atmosphere;
DOI:10.1002/ejoc.201301781

Reference yield:

: C₁₉H₂₁N₃O₈

: 1608113-79-6
C₃₇H₄₆N₅O₁₅P

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium hydrogencarbonate / tetrahydrofuran; water / 16 h / 0 - 20 °C / Inert atmosphere

2.1: palladium 10% on activated carbon; hydrogen / methanol / 16 h / 0 - 20 °C / 760.05 Torr

3.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / dichloromethane / 24 h / 20 °C / Inert atmosphere

4.1: triethylamine tris(hydrogen fluoride) / tetrahydrofuran / 36 h / 20 °C / Inert atmosphere

5.1: 1H-tetrazole / dichloromethane; acetonitrile / 12 h / 0 - 20 °C / Inert atmosphere

5.2: 2 h / -40 - 20 °C / Inert atmosphere

With 1H-tetrazole; palladium 10% on activated carbon; hydrogen; sodium hydrogencarbonate; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine tris(hydrogen fluoride); In tetrahydrofuran; methanol; dichloromethane; water; acetonitrile;
DOI:10.1002/ejoc.201301781

Reference yield:

: 13574-13-5
Boc-Glu(OBzl)-OH

: 1608113-79-6
C₃₇H₄₆N₅O₁₅P

Guidance literature:: Multi-step reaction with 8 steps

1.1: methyl-phenyl-thioether / dichloromethane

2.1: sodium hydrogencarbonate / tetrahydrofuran; water / 16 h / 0 - 20 °C / Inert atmosphere

3.1: dicyclohexyl-carbodiimide / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

4.1: sodium hydrogencarbonate / tetrahydrofuran; water / 16 h / 0 - 20 °C / Inert atmosphere

5.1: palladium 10% on activated carbon; hydrogen / methanol / 16 h / 0 - 20 °C / 760.05 Torr

6.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / dichloromethane / 24 h / 20 °C / Inert atmosphere

7.1: triethylamine tris(hydrogen fluoride) / tetrahydrofuran / 36 h / 20 °C / Inert atmosphere

8.1: 1H-tetrazole / dichloromethane; acetonitrile / 12 h / 0 - 20 °C / Inert atmosphere

8.2: 2 h / -40 - 20 °C / Inert atmosphere

With 1H-tetrazole; methyl-phenyl-thioether; palladium 10% on activated carbon; hydrogen; sodium hydrogencarbonate; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine tris(hydrogen fluoride); dicyclohexyl-carbodiimide; In tetrahydrofuran; methanol; dichloromethane; water; acetonitrile;
DOI:10.1002/ejoc.201301781