N-(N-tert-butoxycarbonylpiperidin-4-ylmethyl), N-({2-[(4-cyanophenyl)-(3-methyl-3H-imidazol-4-ylmethyl)-amino]-ethyl})-2-bromobenzenesulfonamide

Base Information

• Chemical Name: N-(N-tert-butoxycarbonylpiperidin-4-ylmethyl), N-({2-[(4-cyanophenyl)-(3-methyl-3H-imidazol-4-ylmethyl)-amino]-ethyl})-2-bromobenzenesulfonamide
• CAS No.: 1186615-58-6
• Molecular Formula: C₃₁H₃₉BrN₆O₄S
• Molecular Weight: 671.658

Synonyms:N-(N-tert-butoxycarbonylpiperidin-4-ylmethyl), N-({2-[(4-cyanophenyl)-(3-methyl-3H-imidazol-4-ylmethyl)-amino]-ethyl})-2-bromobenzenesulfonamide

Chemical Property of N-(N-tert-butoxycarbonylpiperidin-4-ylmethyl), N-({2-[(4-cyanophenyl)-(3-methyl-3H-imidazol-4-ylmethyl)-amino]-ethyl})-2-bromobenzenesulfonamide

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Technology Process of N-(N-tert-butoxycarbonylpiperidin-4-ylmethyl), N-({2-[(4-cyanophenyl)-(3-methyl-3H-imidazol-4-ylmethyl)-amino]-ethyl})-2-bromobenzenesulfonamide

There total 1 articles about N-(N-tert-butoxycarbonylpiperidin-4-ylmethyl), N-({2-[(4-cyanophenyl)-(3-methyl-3H-imidazol-4-ylmethyl)-amino]-ethyl})-2-bromobenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

4-[(2-(N-tert-butoxycarbonylpiperidin-4-ylmethyl)-aminoethyl)-(3-methyl-3H-imidazol-4-ylmethyl)-amino]-benzonitrile (1186615-62-2) + o-bromobenzenesulfonyl chloride (2905-25-1) → N-(N-tert-butoxycarbonylpiperidin-4-ylmethyl), N-({2-[(4-cyanophenyl)-(3-methyl-3H-imidazol-4-ylmethyl)-amino]-ethyl})-2-bromobenzenesulfonamide (1186615-58-6)

Guidance literature:

In N,N-dimethyl-formamide; at 20 ℃; Cooling with ice; Inert atmosphere;

DOI:10.1016/j.chembiol.2009.01.014

Reference yield: 61.0%

3-(2-methoxycarbonylethyl)phenylboronic acid, (833472-82-5) + N-(N-tert-butoxycarbonylpiperidin-4-ylmethyl), N-({2-[(4-cyanophenyl)-(3-methyl-3H-imidazol-4-ylmethyl)-amino]-ethyl})-2-bromobenzenesulfonamide (1186615-58-6) → N-(N-tert-butoxycarbonylpiperidin-4-ylmethyl), N-({2-[(4-cyanophenyl)-(3-methyl-3H-imidazol-4-ylmethyl)-amino]-ethyl})(3'-(2-methoxycarbonylethyl)-biphenyl)-2-sulfonamide

Guidance literature:

In N,N-dimethyl-formamide; at 110 ℃; for 16h; Inert atmosphere;

DOI:10.1016/j.chembiol.2009.01.014

upstream raw materials:

4-[(2-(N-tert-butoxycarbonylpiperidin-4-ylmethyl)-aminoethyl)-(3-methyl-3H-imidazol-4-ylmethyl)-amino]-benzonitrile

o-bromobenzenesulfonyl chloride

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