5-<(benzyloxycarbonyl)amino>pentyl O-<2,3-di-O-benzoyl-4,6-O-<(R)-1-(methoxycarbonyl)ethylidene>-β-D-galactopyranosyl>-(1<*>3)-2-O-benzoyl-4,6-O-<(S)-1-(methoxycarbonyl)ethylidene>-β-D-glucopyranoside

Base Information

Chemical Name:5-<(benzyloxycarbonyl)amino>pentyl O-<2,3-di-O-benzoyl-4,6-O-<(R)-1-(methoxycarbonyl)ethylidene>-β-D-galactopyranosyl>-(1<*>3)-2-O-benzoyl-4,6-O-<(S)-1-(methoxycarbonyl)ethylidene>-β-D-glucopyranoside
CAS No.:161761-99-5
Molecular Formula:C₅₄H₅₉NO₂₀
Molecular Weight:1042.06
Hs Code.:

5-<(benzyloxycarbonyl)amino>pentyl O-<2,3-di-O-benzoyl-4,6-O-<(R)-1-(methoxycarbonyl)ethylidene>-β-D-galactopyranosyl>-(1<*>3)-2-O-benzoyl-4,6-O-<(S)-1-(methoxycarbonyl)ethylidene>-β-D-glucopyranoside

Synonyms:5-<(benzyloxycarbonyl)amino>pentyl O-<2,3-di-O-benzoyl-4,6-O-<(R)-1-(methoxycarbonyl)ethylidene>-β-D-galactopyranosyl>-(1<*>3)-2-O-benzoyl-4,6-O-<(S)-1-(methoxycarbonyl)ethylidene>-β-D-glucopyranoside

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Chemical Property of 5-<(benzyloxycarbonyl)amino>pentyl O-<2,3-di-O-benzoyl-4,6-O-<(R)-1-(methoxycarbonyl)ethylidene>-β-D-galactopyranosyl>-(1<*>3)-2-O-benzoyl-4,6-O-<(S)-1-(methoxycarbonyl)ethylidene>-β-D-glucopyranoside

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Technology Process of 5-<(benzyloxycarbonyl)amino>pentyl O-<2,3-di-O-benzoyl-4,6-O-<(R)-1-(methoxycarbonyl)ethylidene>-β-D-galactopyranosyl>-(1<*>3)-2-O-benzoyl-4,6-O-<(S)-1-(methoxycarbonyl)ethylidene>-β-D-glucopyranoside

There total 1 articles about 5-<(benzyloxycarbonyl)amino>pentyl O-<2,3-di-O-benzoyl-4,6-O-<(R)-1-(methoxycarbonyl)ethylidene>-β-D-galactopyranosyl>-(1<*>3)-2-O-benzoyl-4,6-O-<(S)-1-(methoxycarbonyl)ethylidene>-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

: 87905-98-4
5-<(benzyloxycarbonyl)amino>pentanol

: O-<2,3-di-O-benzoyl-4,6-O-<(R)-1-(methoxycarbonyl)ethylidene>-β-D-galactopyranosyl>-(1<*>3)-2-O-benzoyl-4,6-O-<(S)-1-(methoxycarbonyl)ethylidene>-D-glucopyranosyl trichloroacetimidate

: 161761-99-5
5-<(benzyloxycarbonyl)amino>pentyl O-<2,3-di-O-benzoyl-4,6-O-<(R)-1-(methoxycarbonyl)ethylidene>-β-D-galactopyranosyl>-(1<*>3)-2-O-benzoyl-4,6-O-<(S)-1-(methoxycarbonyl)ethylidene>-β-D-glucopyranoside

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at -20 ℃; for 1h;
DOI:10.1016/S0008-6215(05)80010-2

Reference yield:

: 161761-99-5
5-<(benzyloxycarbonyl)amino>pentyl O-<2,3-di-O-benzoyl-4,6-O-<(R)-1-(methoxycarbonyl)ethylidene>-β-D-galactopyranosyl>-(1<*>3)-2-O-benzoyl-4,6-O-<(S)-1-(methoxycarbonyl)ethylidene>-β-D-glucopyranoside

: C₃₃H₄₇NO₁₇

Guidance literature:: With sodium methylate; In methanol; toluene; for 24h; Ambient temperature;
DOI:10.1016/S0008-6215(05)80010-2

Reference yield:

: 161761-99-5
5-<(benzyloxycarbonyl)amino>pentyl O-<2,3-di-O-benzoyl-4,6-O-<(R)-1-(methoxycarbonyl)ethylidene>-β-D-galactopyranosyl>-(1<*>3)-2-O-benzoyl-4,6-O-<(S)-1-(methoxycarbonyl)ethylidene>-β-D-glucopyranoside

: C₃₁H₄₃NO₁₇

Guidance literature:: Multi-step reaction with 2 steps

1: NaOMe / toluene; methanol / 24 h / Ambient temperature

2: aq. NaOH / methanol / 3 h / 40 °C

With sodium hydroxide; sodium methylate; In methanol; toluene;
DOI:10.1016/S0008-6215(05)80010-2