allyl 4-O-acetyl-6-O-benzyl-2-deoxy-3-O-levulinoyl-2-trichloroacetamido-β-D-glucopyranoside

Base Information

Chemical Name:allyl 4-O-acetyl-6-O-benzyl-2-deoxy-3-O-levulinoyl-2-trichloroacetamido-β-D-glucopyranoside
CAS No.:765910-46-1
Molecular Formula:C₂₅H₃₀Cl₃NO₉
Molecular Weight:594.874
Hs Code.:

Synonyms:allyl 4-O-acetyl-6-O-benzyl-2-deoxy-3-O-levulinoyl-2-trichloroacetamido-β-D-glucopyranoside

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Chemical Property of allyl 4-O-acetyl-6-O-benzyl-2-deoxy-3-O-levulinoyl-2-trichloroacetamido-β-D-glucopyranoside

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Technology Process of allyl 4-O-acetyl-6-O-benzyl-2-deoxy-3-O-levulinoyl-2-trichloroacetamido-β-D-glucopyranoside

There total 8 articles about allyl 4-O-acetyl-6-O-benzyl-2-deoxy-3-O-levulinoyl-2-trichloroacetamido-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 108-24-7
acetic anhydride

: 765910-31-4
allyl 6-O-benzyl-2-deoxy-3-O-levulinoyl-2-trichloroacetamido-β-D-glucopyranoside

: 765910-46-1
allyl 4-O-acetyl-6-O-benzyl-2-deoxy-3-O-levulinoyl-2-trichloroacetamido-β-D-glucopyranoside

Guidance literature:: With dmap; In dichloromethane; at 0 - 20 ℃; for 1h; Inert atmosphere;
DOI:10.1002/adsc.201000008

Reference yield:

: allyl 4,6-O-benzylidene-2-deoxy-2-trichloroacetamido-β-D-glucopyranoside

: 765910-46-1
allyl 4-O-acetyl-6-O-benzyl-2-deoxy-3-O-levulinoyl-2-trichloroacetamido-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 98 percent / DMAP; diisopropylcarbodiimide / CH₂Cl₂ / 13 h / 0 - 20 °C

2: 72 percent / Et₃SiH; trifluoroacetic acid anhydride; CF₃CO₂H / CH₂Cl₂ / 10 h / 0 °C

3: 1.82 g / DMAP / CH₂Cl₂ / 1 h

With triethylsilane; dmap; trifluoroacetic acid; trifluoroacetic anhydride; diisopropyl-carbodiimide; In dichloromethane;
DOI:10.1016/j.tet.2004.06.037

Reference yield:

: 765910-45-0
allyl 4,6-O-benzylidene-2-deoxy-3-O-levulinoyl-2-trichloroacetamido-β-D-glucopyranoside

: 765910-46-1
allyl 4-O-acetyl-6-O-benzyl-2-deoxy-3-O-levulinoyl-2-trichloroacetamido-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 72 percent / Et₃SiH; trifluoroacetic acid anhydride; CF₃CO₂H / CH₂Cl₂ / 10 h / 0 °C

2: 1.82 g / DMAP / CH₂Cl₂ / 1 h

With triethylsilane; dmap; trifluoroacetic acid; trifluoroacetic anhydride; In dichloromethane;
DOI:10.1016/j.tet.2004.06.037