phenyl 2,3,6-tri-O-benzyl-4-O-(2-carboxybenzoyl)-1-thio-β-D-galactopyranoside

Base Information

Chemical Name:phenyl 2,3,6-tri-O-benzyl-4-O-(2-carboxybenzoyl)-1-thio-β-D-galactopyranoside
CAS No.:1083237-08-4
Molecular Formula:C₄₁H₃₈O₈S
Molecular Weight:690.814
Hs Code.:

Synonyms:phenyl 2,3,6-tri-O-benzyl-4-O-(2-carboxybenzoyl)-1-thio-β-D-galactopyranoside

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Chemical Property of phenyl 2,3,6-tri-O-benzyl-4-O-(2-carboxybenzoyl)-1-thio-β-D-galactopyranoside

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Technology Process of phenyl 2,3,6-tri-O-benzyl-4-O-(2-carboxybenzoyl)-1-thio-β-D-galactopyranoside

There total 1 articles about phenyl 2,3,6-tri-O-benzyl-4-O-(2-carboxybenzoyl)-1-thio-β-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

: 85-44-9
phthalic anhydride

: 144781-45-3
phenyl 2,3,6-tri-O-benzyl-1-thio-β-D-galactopyranoside

: 1083237-08-4
phenyl 2,3,6-tri-O-benzyl-4-O-(2-carboxybenzoyl)-1-thio-β-D-galactopyranoside

Guidance literature:: phenyl 2,3,6-tri-O-benzyl-1-thio-β-D-galactopyranoside; With sodium hydride; In N,N-dimethyl-formamide; at 20 ℃; for 0.166667h; Inert atmosphere;

phthalic anhydride; In N,N-dimethyl-formamide; at 20 ℃; Inert atmosphere;
DOI:10.1021/jo801630m

Reference yield: 93.0%

: 1083237-08-4
phenyl 2,3,6-tri-O-benzyl-4-O-(2-carboxybenzoyl)-1-thio-β-D-galactopyranoside

: 100-09-4
4-methoxybenzoic acid

: 1083237-11-9
phenyl 2,3,6-tri-O-benzyl-4-O-(4-methoxybenzoyl)-1-thio-β-D-galactopyranoside

Guidance literature:: 4-methoxybenzoic acid; With 1,1'-carbonyldiimidazole; In acetonitrile; at 60 - 70 ℃; for 2h; Inert atmosphere;

phenyl 2,3,6-tri-O-benzyl-4-O-(2-carboxybenzoyl)-1-thio-β-D-galactopyranoside; With 1,8-diazabicyclo[5.4.0]undec-7-ene; In acetonitrile; at 60 ℃; Inert atmosphere;
DOI:10.1021/jo801630m

Reference yield: 41.0%

: 1083237-08-4
phenyl 2,3,6-tri-O-benzyl-4-O-(2-carboxybenzoyl)-1-thio-β-D-galactopyranoside

: 1083237-10-8
3,4,6-tri-O-benzyl-1,4-O-phthaloyl-α-D-galactopyranose

Guidance literature:: phenyl 2,3,6-tri-O-benzyl-4-O-(2-carboxybenzoyl)-1-thio-β-D-galactopyranoside; With N-iodo-succinimide; In dichloromethane; Molecular sieve; Inert atmosphere; Cooling;

With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at -30 ℃; Inert atmosphere;
DOI:10.1021/jo801630m