C₄₁H₄₇NO₈

Base Information

Chemical Name:C₄₁H₄₇NO₈
CAS No.:1379450-04-0
Molecular Formula:C₄₁H₄₇NO₈
Molecular Weight:681.826
Hs Code.:

C<sub>41</sub>H<sub>47</sub>NO<sub>8</sub>

Synonyms:C₄₁H₄₇NO₈

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Chemical Property of C₄₁H₄₇NO₈

Chemical Property:

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Technology Process of C₄₁H₄₇NO₈

There total 10 articles about C₄₁H₄₇NO₈ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1379449-92-9
C₄₇H₆₁NO₈Si

: 1379450-04-0
C₄₁H₄₇NO₈

Guidance literature:: With pyridine; pyridine hydrogenfluoride; In tetrahydrofuran; at 0 - 25 ℃; Inert atmosphere;
DOI:10.1021/ja301326k

Reference yield:

: 1379449-94-1
C₂₁H₃₂N₂O₆

: 1379450-04-0
C₄₁H₄₇NO₈

Guidance literature:: Multi-step reaction with 7 steps

1: tetrahydrofuran / -78 - 0 °C / Inert atmosphere

2: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / dichloromethane / 12 h / 25 °C

3: tetrahydrofuran / 0 - 25 °C / Inert atmosphere; Molecular sieve

4: pyridinium chlorochromate / dichloromethane / 4 h / 25 °C / Inert atmosphere; Molecular sieve

5: 2,6-di-tert-butyl-pyridine / nitromethane / 2 h / -20 °C / Inert atmosphere; Molecular sieve

6: copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; Tetrabutylammoniumsalz der Diphenylphosphinsaeure / N,N-dimethyl-formamide / 16 h / 45 °C / Inert atmosphere

7: pyridine; pyridine hydrogenfluoride / tetrahydrofuran / 0 - 25 °C / Inert atmosphere

With pyridine; tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; 2,6-di-tert-butyl-pyridine; pyridine hydrogenfluoride; Tetrabutylammoniumsalz der Diphenylphosphinsaeure; pyridinium chlorochromate; In tetrahydrofuran; nitromethane; dichloromethane; N,N-dimethyl-formamide; 5: Friedel Crafts acylation / 6: Stille coupling;
DOI:10.1021/ja301326k

Reference yield:

: 1379449-81-6
C₁₈H₂₈N₂O₆

: 1379450-04-0
C₄₁H₄₇NO₈

Guidance literature:: Multi-step reaction with 8 steps

1.1: sodium hydride / N,N-dimethyl-formamide / 1 h / 0 °C

1.2: 6 h / 0 °C

2.1: tetrahydrofuran / -78 - 0 °C / Inert atmosphere

3.1: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / dichloromethane / 12 h / 25 °C

4.1: tetrahydrofuran / 0 - 25 °C / Inert atmosphere; Molecular sieve

5.1: pyridinium chlorochromate / dichloromethane / 4 h / 25 °C / Inert atmosphere; Molecular sieve

6.1: 2,6-di-tert-butyl-pyridine / nitromethane / 2 h / -20 °C / Inert atmosphere; Molecular sieve

7.1: copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; Tetrabutylammoniumsalz der Diphenylphosphinsaeure / N,N-dimethyl-formamide / 16 h / 45 °C / Inert atmosphere

8.1: pyridine; pyridine hydrogenfluoride / tetrahydrofuran / 0 - 25 °C / Inert atmosphere

With pyridine; tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; 2,6-di-tert-butyl-pyridine; sodium hydride; pyridine hydrogenfluoride; Tetrabutylammoniumsalz der Diphenylphosphinsaeure; pyridinium chlorochromate; In tetrahydrofuran; nitromethane; dichloromethane; N,N-dimethyl-formamide; 6.1: Friedel Crafts acylation / 7.1: Stille coupling;
DOI:10.1021/ja301326k