endo-N-[(1S,2S)-1,3-dihydroxy-1-phenylprop-2-yl]bicyclo[2.2.1]hept-5-ene-2,3-dicarboximide

Base Information

• Chemical Name: endo-N-[(1S,2S)-1,3-dihydroxy-1-phenylprop-2-yl]bicyclo[2.2.1]hept-5-ene-2,3-dicarboximide
• CAS No.: 1009375-31-8
• Molecular Formula: C₁₈H₁₉NO₄
• Molecular Weight: 313.353

Synonyms:endo-N-[(1S,2S)-1,3-dihydroxy-1-phenylprop-2-yl]bicyclo[2.2.1]hept-5-ene-2,3-dicarboximide

Chemical Property of endo-N-[(1S,2S)-1,3-dihydroxy-1-phenylprop-2-yl]bicyclo[2.2.1]hept-5-ene-2,3-dicarboximide

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Technology Process of endo-N-[(1S,2S)-1,3-dihydroxy-1-phenylprop-2-yl]bicyclo[2.2.1]hept-5-ene-2,3-dicarboximide

There total 1 articles about endo-N-[(1S,2S)-1,3-dihydroxy-1-phenylprop-2-yl]bicyclo[2.2.1]hept-5-ene-2,3-dicarboximide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

(1S,2S)-2-amino-1-phenyl-1,3-diol (28143-91-1) + 3,6-endomethylene-1,2,3,6-tetrahydrophthalic anhydride (129-64-6) → endo-N-[(1S,2S)-1,3-dihydroxy-1-phenylprop-2-yl]bicyclo[2.2.1]hept-5-ene-2,3-dicarboximide (1009375-31-8)

Guidance literature:

In toluene; at 80 ℃;

DOI:10.1039/b713449e

Reference yield: 97.0%

endo-N-[(1S,2S)-1,3-dihydroxy-1-phenylprop-2-yl]bicyclo[2.2.1]hept-5-ene-2,3-dicarboximide (1009375-31-8) → C18H23NO2 (1009375-28-3)

Guidance literature:

With lithium aluminium tetrahydride; In tetrahydrofuran; for 48h; Heating;

DOI:10.1039/b713449e

Reference yield: 71.0%

endo-N-[(1S,2S)-1,3-dihydroxy-1-phenylprop-2-yl]bicyclo[2.2.1]hept-5-ene-2,3-dicarboximide (1009375-31-8) + 3,3',5,5'-tetra-tert-butyl-1,1'-biphenyl-2,2'-diyl phosphorochloridite (71941-98-5) → endo-N-[(1S,2S)-1,3-bis(3,3',5,5'-tetrakis(tert-butyl)biphenyl-2,2'-diylphosphito)-1-phenylprop-2-yl]bicyclo[2.2.1]hept-5-ene-2,3-dicarboximide (1236034-54-0)

Guidance literature:

With pyridine; In toluene; at 0 - 20 ℃; Inert atmosphere;

DOI:10.1002/ejic.200900879

upstream raw materials:

(1S,2S)-2-amino-1-phenyl-1,3-diol

3,6-endomethylene-1,2,3,6-tetrahydrophthalic anhydride

Downstream raw materials:

C₁₈H₂₃NO₂

endo-N-[(1S,2S)-1,3-bis(3,3',5,5'-tetrakis(tert-butyl)biphenyl-2,2'-diylphosphito)-1-phenylprop-2-yl]bicyclo[2.2.1]hept-5-ene-2,3-dicarboximide

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