6-p-Chlorophenyl-5,6-dihydro-1-phenyl-1H,4H-pyrazolo<4,3-f>pyrrolo<1,2-a><1,4>diazepine Hydrochloride

Base Information

• Chemical Name: 6-p-Chlorophenyl-5,6-dihydro-1-phenyl-1H,4H-pyrazolo<4,3-f>pyrrolo<1,2-a><1,4>diazepine Hydrochloride
• CAS No.: 95834-41-6
• Molecular Formula: C₂₁H₁₇ClN₄*ClH
• Molecular Weight: 397.307

Synonyms:6-p-Chlorophenyl-5,6-dihydro-1-phenyl-1H,4H-pyrazolo<4,3-f>pyrrolo<1,2-a><1,4>diazepine Hydrochloride

Chemical Property of 6-p-Chlorophenyl-5,6-dihydro-1-phenyl-1H,4H-pyrazolo<4,3-f>pyrrolo<1,2-a><1,4>diazepine Hydrochloride

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Technology Process of 6-p-Chlorophenyl-5,6-dihydro-1-phenyl-1H,4H-pyrazolo<4,3-f>pyrrolo<1,2-a><1,4>diazepine Hydrochloride

There total 4 articles about 6-p-Chlorophenyl-5,6-dihydro-1-phenyl-1H,4H-pyrazolo<4,3-f>pyrrolo<1,2-a><1,4>diazepine Hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

4-p-Chlorbenzylideneaminomethyl-1-phenyl-5-(1-pyrryl)pyrazole (95834-38-1) → 6-p-Chlorophenyl-5,6-dihydro-1-phenyl-1H,4H-pyrazolo<4,3-f>pyrrolo<1,2-a><1,4>diazepine Hydrochloride (95834-41-6)

Guidance literature:

With hydrogenchloride; In ethanol; for 0.5h; Heating;

DOI:10.1002/jhet.5570210658

Reference yield:

5-Amino-4-cyano-1-phenylpyrazole (5334-43-0) → 6-p-Chlorophenyl-5,6-dihydro-1-phenyl-1H,4H-pyrazolo<4,3-f>pyrrolo<1,2-a><1,4>diazepine Hydrochloride (95834-41-6)

Guidance literature:

Multi-step reaction with 4 steps

1: 93 percent / acetic acid / 0.5 h / Heating

2: 80 percent / LiAlH₄ / tetrahydrofuran / 18 h / Ambient temperature

3: 83 percent / ethanol / 0.17 h / Heating

4: 77 percent / HCl gas / ethanol / 0.5 h / Heating

With hydrogenchloride; lithium aluminium tetrahydride; In tetrahydrofuran; ethanol; acetic acid;

DOI:10.1002/jhet.5570210658

Reference yield:

4-Cyano-1-phenyl-5-(1-pyrryl)pyrazole (95834-35-8) → 6-p-Chlorophenyl-5,6-dihydro-1-phenyl-1H,4H-pyrazolo<4,3-f>pyrrolo<1,2-a><1,4>diazepine Hydrochloride (95834-41-6)

Guidance literature:

Multi-step reaction with 3 steps

1: 80 percent / LiAlH₄ / tetrahydrofuran / 18 h / Ambient temperature

2: 83 percent / ethanol / 0.17 h / Heating

3: 77 percent / HCl gas / ethanol / 0.5 h / Heating

With hydrogenchloride; lithium aluminium tetrahydride; In tetrahydrofuran; ethanol;

DOI:10.1002/jhet.5570210658

upstream raw materials:

4-p-Chlorbenzylideneaminomethyl-1-phenyl-5-(1-pyrryl)pyrazole

5-Amino-4-cyano-1-phenylpyrazole

4-Cyano-1-phenyl-5-(1-pyrryl)pyrazole

4-Aminomethyl-1-phenyl-5-(1-pyrryl)pyrazole

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