(4Z,9Z)-1,15,21,24-tetrahydro-19-(4-methoxybenzoyl)-15-hydroxy-5,10,15-tris(4-methoxyphenyl)-23H-bilin-1-one

Base Information

• Chemical Name: (4Z,9Z)-1,15,21,24-tetrahydro-19-(4-methoxybenzoyl)-15-hydroxy-5,10,15-tris(4-methoxyphenyl)-23H-bilin-1-one
• CAS No.: 130471-42-0
• Molecular Formula: C₄₈H₄₀N₄O₇
• Molecular Weight: 784.868
• Mol file: 130471-42-0.mol

Synonyms:(4Z,9Z)-1,15,21,24-tetrahydro-19-(4-methoxybenzoyl)-15-hydroxy-5,10,15-tris(4-methoxyphenyl)-23H-bilin-1-one

Chemical Property of (4Z,9Z)-1,15,21,24-tetrahydro-19-(4-methoxybenzoyl)-15-hydroxy-5,10,15-tris(4-methoxyphenyl)-23H-bilin-1-one

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (4Z,9Z)-1,15,21,24-tetrahydro-19-(4-methoxybenzoyl)-15-hydroxy-5,10,15-tris(4-methoxyphenyl)-23H-bilin-1-one

There total 4 articles about (4Z,9Z)-1,15,21,24-tetrahydro-19-(4-methoxybenzoyl)-15-hydroxy-5,10,15-tris(4-methoxyphenyl)-23H-bilin-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

(C20H8N4(C6H4OCH3)4)FeCl (36995-20-7,333460-15-4) → (4Z,9Z,15Z)-5,10,15-tri(4-methoxyphenyl)-(21H,23H,24H)-1,19,21,24-tetrahydro-1,19-bilindione (1314046-37-1) + (4Z,9Z)-1,15,21,24-tetrahydro-19-(4-methoxybenzoyl)-15-hydroxy-5,10,15-tris(4-methoxyphenyl)-23H-bilin-1-one (130471-42-0)

Guidance literature:

(C₂₀H₈N₄(C₆H₄OCH₃)4)FeCl; With pyridine; oxygen; ascorbic acid; In chloroform;

With hydrogenchloride; In chloroform; water;

DOI:10.1142/S1088424615500455

Reference yield: 84.7%

[5,10,15,20-tetrakis(4-methoxyphenyl)porphirinato]iron(III) chloride → (4Z,9Z)-1,15,21,24-tetrahydro-19-(4-methoxybenzoyl)-15-hydroxy-5,10,15-tris(4-methoxyphenyl)-23H-bilin-1-one (130471-42-0)

Guidance literature:

[5,10,15,20-tetrakis(4-methoxyphenyl)porphirinato]iron(III) chloride; With pyridine; oxygen; ascorbic acid; In chloroform; at 24.84 ℃; for 1h;

With hydrogenchloride; In chloroform; at 20 ℃; for 1h; Further stages.;

DOI:10.1021/jo070692a

Reference yield:

[5,10,15,20-tetra(4-methoxyphenyl)porphyrinato]iron(III) chloride → (4Z,9Z)-1,15,21,24-tetrahydro-19-(4-methoxybenzoyl)-15-hydroxy-5,10,15-tris(4-methoxyphenyl)-23H-bilin-1-one (130471-42-0)

Guidance literature:

[5,10,15,20-tetra(4-methoxyphenyl)porphyrinato]iron(III) chloride; With pyridine; oxygen; ascorbic acid; In chloroform; at 20 ℃; for 4h;

With hydrogenchloride; In chloroform; water; for 2h;

DOI:10.1021/jo2007994

upstream raw materials:

5,10,15,20-tetrakis(4-methoxyphenyl)porphyrin

(C₂₀H₈N₄(C₆H₄OCH₃)4)FeCl