C₁₂H₁₂O₃⁽¹⁸⁾O

Base Information

Chemical Name:C₁₂H₁₂O₃⁽¹⁸⁾O
CAS No.:1340589-23-2
Molecular Formula:C₁₂H₁₂O₄
Molecular Weight:222.225
Hs Code.:

C<sub>12</sub>H<sub>12</sub>O<sub>3</sub><sup>(18)</sup>O

Synonyms:C₁₂H₁₂O₃⁽¹⁸⁾O

Suppliers and Price of C₁₂H₁₂O₃⁽¹⁸⁾O

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₂H₁₂O₃⁽¹⁸⁾O

Chemical Property:

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Technology Process of C₁₂H₁₂O₃⁽¹⁸⁾O

There total 2 articles about C₁₂H₁₂O₃⁽¹⁸⁾O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1330064-93-1
[C₁-⁽¹⁸⁾O]-3-benzyl-2-hydroxy-cyclopent-2-en-1-one

: 1340589-23-2
C₁₂H₁₂O₃⁽¹⁸⁾O

Guidance literature:: [C₁-⁽¹⁸⁾O]-3-benzyl-2-hydroxy-cyclopent-2-en-1-one; With titanium(IV) isopropylate; tert.-butylhydroperoxide; diethyl (2R,3R)-tartrate; In dichloromethane; at -20 ℃; for 68.33h; Inert atmosphere; Molecular sieve;

In toluene; at 100 ℃; for 2h; Mechanism; Inert atmosphere;
DOI:10.1016/j.tet.2011.06.036

Reference yield:

: 25684-06-4
2-hydroxy-3-(benzyl)-2-cyclopenten-1-one

: 1340589-23-2
C₁₂H₁₂O₃⁽¹⁸⁾O

Guidance literature:: Multi-step reaction with 2 steps

1.1: hydrogenchloride; ¹⁸O-labeled water / 1,4-dioxane; 1,4-dioxane-d8 / 60 h / 20 °C

2.1: titanium(IV) isopropylate; tert.-butylhydroperoxide; diethyl (2R,3R)-tartrate / dichloromethane / 68.33 h / -20 °C / Inert atmosphere; Molecular sieve

2.2: 2 h / 100 °C / Inert atmosphere

With titanium(IV) isopropylate; hydrogenchloride; tert.-butylhydroperoxide; diethyl (2R,3R)-tartrate; ¹⁸O-labeled water; In 1,4-dioxane; 1,4-dioxane-d8; dichloromethane;
DOI:10.1016/j.tet.2011.06.036