6-benzyloxy-9-[(2S,4R)-4-acetoxy-N-(methoxycarbonyl)-2-pyrrolidinyl]purine

Base Information

Chemical Name:6-benzyloxy-9-[(2S,4R)-4-acetoxy-N-(methoxycarbonyl)-2-pyrrolidinyl]purine
CAS No.:1007228-92-3
Molecular Formula:C₂₀H₂₁N₅O₅
Molecular Weight:411.417
Hs Code.:

Synonyms:6-benzyloxy-9-[(2S,4R)-4-acetoxy-N-(methoxycarbonyl)-2-pyrrolidinyl]purine

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Chemical Property of 6-benzyloxy-9-[(2S,4R)-4-acetoxy-N-(methoxycarbonyl)-2-pyrrolidinyl]purine

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Technology Process of 6-benzyloxy-9-[(2S,4R)-4-acetoxy-N-(methoxycarbonyl)-2-pyrrolidinyl]purine

There total 2 articles about 6-benzyloxy-9-[(2S,4R)-4-acetoxy-N-(methoxycarbonyl)-2-pyrrolidinyl]purine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 34.0%

: 279671-69-1
(2S,4R)-4-(acetyloxy)-1-(methoxycarbonyl)-2-pyrrolidinecarboxylic acid

: 1007228-93-4
6-benzyloxy-9-[(2R,4R)-4-acetoxy-N-(methoxycarbonyl)-2-pyrrolidinyl]purine

: 1007228-92-3
6-benzyloxy-9-[(2S,4R)-4-acetoxy-N-(methoxycarbonyl)-2-pyrrolidinyl]purine

Guidance literature:: (2S,4R)-4-(acetyloxy)-1-(methoxycarbonyl)-2-pyrrolidinecarboxylic acid; With [bis(acetoxy)iodo]benzene; In dichloromethane; at 25 ℃; for 3h; visible light irradiation;

With methanol; In dichloromethane; at 25 ℃; for 0.5h;

7⁽⁹⁾-trimethylsilyl-6-benzyloxypurine; With boron trifluoride diethyl etherate; In acetonitrile; at 0 ℃; for 1h; diastereoselective reaction;
DOI:10.1002/ejoc.201000360

Reference yield: 34.0%

: C₁₅H₁₈N₄OSi

: 279671-69-1
(2S,4R)-4-(acetyloxy)-1-(methoxycarbonyl)-2-pyrrolidinecarboxylic acid

: 1007228-93-4
6-benzyloxy-9-[(2R,4R)-4-acetoxy-N-(methoxycarbonyl)-2-pyrrolidinyl]purine

: 1007228-92-3
6-benzyloxy-9-[(2S,4R)-4-acetoxy-N-(methoxycarbonyl)-2-pyrrolidinyl]purine

Guidance literature:: (2S,4R)-4-(acetyloxy)-1-(methoxycarbonyl)-2-pyrrolidinecarboxylic acid; With [bis(acetoxy)iodo]benzene; iodine; In dichloromethane; at 25 ℃; for 3h;

With methanol; In dichloromethane; at 25 ℃; for 0.5h;

C₁₅H₁₈N₄OSi; With boron trifluoride diethyl etherate; In acetonitrile; at 0 ℃; for 1h; Further stages.;
DOI:10.1016/j.tetlet.2007.11.113