1-phenyl-1-benzarsole

Base Information

Chemical Name:1-phenyl-1-benzarsole
CAS No.:152554-98-8
Molecular Formula:C₁₄H₁₁As
Molecular Weight:254.163
Hs Code.:

Synonyms:1-phenyl-1-benzarsole

Suppliers and Price of 1-phenyl-1-benzarsole

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-phenyl-1-benzarsole

Chemical Property:

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Technology Process of 1-phenyl-1-benzarsole

There total 11 articles about 1-phenyl-1-benzarsole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 152554-91-1
1-phenyl-2-trimethylsilylbenzo[b]arsole

: 152554-98-8
1-phenyl-1-benzarsole

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; for 2h; Heating;
DOI:10.1248/cpb.42.1437

Reference yield:

: 2170-06-1
1-Phenyl-2-(trimethylsilyl)acetylene

: 152554-98-8
1-phenyl-1-benzarsole

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) DIBAL-H, 2.) NBS / 1.) hexane, RT, 10 h, 2.) 0 deg C

2: 1.) BuLi / 1.) ether, hexane, RT, 2 h, 2.) ether, hexane, RT, 20 h

3: 97 percent / TBAF / tetrahydrofuran / 2 h / Heating

With N-Bromosuccinimide; n-butyllithium; tetrabutyl ammonium fluoride; diisobutylaluminium hydride; In tetrahydrofuran;
DOI:10.1248/cpb.42.1437

Reference yield:

: 583-55-1
1-Bromo-2-iodobenzene

: 152554-98-8
1-phenyl-1-benzarsole

Guidance literature:: Multi-step reaction with 4 steps

1: 91 percent / Pd(PPh₃)2Cl₂, CuI, Et₂NH / 3.5 h / Ambient temperature

2: 1.) DIBAL-H, 2.) NBS / 1.) hexane, RT, 3 d, 2.) hexane, a) -20 deg C, 30 min, b) RT, 1 h

3: 1.) BuLi / 1.) ether, hexane, RT, 2 h, 2.) ether, hexane, RT, 20 h

4: 97 percent / TBAF / tetrahydrofuran / 2 h / Heating

With bis-triphenylphosphine-palladium(II) chloride; N-Bromosuccinimide; copper(l) iodide; n-butyllithium; tetrabutyl ammonium fluoride; diisobutylaluminium hydride; diethylamine; In tetrahydrofuran;
DOI:10.1248/cpb.42.1437