Technology Process of C14H15(2)HN2O8
There total 8 articles about C14H15(2)HN2O8 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
acetic acid; sodium nitrite;
cetyltributylphosphonium bromide;
In
water; benzene;
for 0.416667h;
Ambient temperature;
DOI:10.1016/S0008-6215(00)85519-6
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 40 percent
2: 72 percent / methanesulfonyl chloride, triethylamine / CH2Cl2 / 15 h / 0 °C
3: 32 percent / sodium nitrite, acetic acid-O-d / tributylhexadecylphosphonium bromide / benzene; D2O / 25 h / Ambient temperature
4: 87 percent / urea, triethylamine / CH2Cl2 / 0.25 h / 0 °C
5: 46 percent / sodium nitrite, acetic acid / tributylhexadecylphosphonium bromide / benzene; H2O / 0.42 h / Ambient temperature
With
deuteroacetic acid; acetic acid; methanesulfonyl chloride; triethylamine; urea; sodium nitrite;
cetyltributylphosphonium bromide;
In
dichloromethane; water; water-d2; benzene;
DOI:10.1016/S0008-6215(00)85519-6
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 58 percent / sodium nitrite / tributylhexadecylphosphonium bromide / benzene; D2O / 2 h / Ambient temperature
2: 46 percent / sodium nitrite, acetic acid / tributylhexadecylphosphonium bromide / benzene; H2O / 0.42 h / Ambient temperature
With
acetic acid; sodium nitrite;
cetyltributylphosphonium bromide;
In
water; water-d2; benzene;
DOI:10.1016/S0008-6215(00)85519-6
