2-C-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)-7-mesyloxy-6-methoxy-1,3-diallyloxyxanthone

Base Information

Chemical Name:2-C-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)-7-mesyloxy-6-methoxy-1,3-diallyloxyxanthone
CAS No.:1239694-48-4
Molecular Formula:C₅₅H₅₄O₁₃S
Molecular Weight:955.092
Hs Code.:

Synonyms:2-C-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)-7-mesyloxy-6-methoxy-1,3-diallyloxyxanthone

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Chemical Property of 2-C-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)-7-mesyloxy-6-methoxy-1,3-diallyloxyxanthone

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Technology Process of 2-C-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)-7-mesyloxy-6-methoxy-1,3-diallyloxyxanthone

There total 1 articles about 2-C-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)-7-mesyloxy-6-methoxy-1,3-diallyloxyxanthone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 1239694-43-9
2-C-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)-7-mesyloxy-6-trimethoxy-1,3-diallylxanthene

: 1239694-48-4
2-C-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)-7-mesyloxy-6-methoxy-1,3-diallyloxyxanthone

Guidance literature:: 2-C-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)-7-mesyloxy-6-trimethoxy-1,3-diallylxanthene; With 2,3-dicyano-5,6-dichloro-p-benzoquinone; In 1,4-dioxane; dichloromethane; water; at 0 - 20 ℃;

With dmap; In 1,4-dioxane; dichloromethane; water; ethyl acetate;
DOI:10.1021/jo100776q

Reference yield: 96.0%

: 1239694-48-4
2-C-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)-7-mesyloxy-6-methoxy-1,3-diallyloxyxanthone

: 1239694-49-5
2-C-(2,3,4,6-tetra-O-benzyl-β-D-glucopyranosyl)-7-mesyloxy-6-methoxy-1,3-dihydroxyxanthone

Guidance literature:: With 1,4-diaza-bicyclo[2.2.2]octane; Wilkinson's catalyst; In ethanol; water; toluene; for 10h; Reflux;
DOI:10.1021/jo100776q