(2S)-2-phenyl-2-propenylcyclopropanone 1,3-(2,2-dimethyl)propanediyl acetal

Base Information

Chemical Name:(2S)-2-phenyl-2-propenylcyclopropanone 1,3-(2,2-dimethyl)propanediyl acetal
CAS No.:288260-63-9
Molecular Formula:C₁₇H₂₂O₂
Molecular Weight:258.36
Hs Code.:

Synonyms:(2S)-2-phenyl-2-propenylcyclopropanone 1,3-(2,2-dimethyl)propanediyl acetal

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Chemical Property of (2S)-2-phenyl-2-propenylcyclopropanone 1,3-(2,2-dimethyl)propanediyl acetal

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Technology Process of (2S)-2-phenyl-2-propenylcyclopropanone 1,3-(2,2-dimethyl)propanediyl acetal

There total 2 articles about (2S)-2-phenyl-2-propenylcyclopropanone 1,3-(2,2-dimethyl)propanediyl acetal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 122762-89-4
2-phenylcyclopropenone 2,2-dimethyl-1,3-propanediyl acetal

: C₂₂H₂₂N₂O₂Zn

: 288260-63-9
(2S)-2-phenyl-2-propenylcyclopropanone 1,3-(2,2-dimethyl)propanediyl acetal

Guidance literature:: In tetrahydrofuran; hexane; at 25 ℃; for 12h; under 7500750 Torr;
DOI:10.1021/ol005892m

Reference yield: 98.0%

: 18925-10-5
allylzinc bromide

: 122762-89-4
2-phenylcyclopropenone 2,2-dimethyl-1,3-propanediyl acetal

: 288260-63-9
(2S)-2-phenyl-2-propenylcyclopropanone 1,3-(2,2-dimethyl)propanediyl acetal

Guidance literature:: allylzinc bromide; With [2,2]bipyridinyl; n-butyllithium; bis-oxazoline derived from (S)-(+)-2-phenylglycinol; In tetrahydrofuran; hexane; at 0 - 20 ℃; for 0.333333h;

2-phenylcyclopropenone 2,2-dimethyl-1,3-propanediyl acetal; In tetrahydrofuran; hexane; at 25 ℃; for 13h; under 7500600 Torr;
DOI:10.1016/S0022-328X(01)00679-9