N-[4-(4,4,5,5-tetramethyl-[1,3,2]-dioxaborolan-2-yl)phenyl]-N'-thiophen-3-ylurea

Base Information

Chemical Name:N-[4-(4,4,5,5-tetramethyl-[1,3,2]-dioxaborolan-2-yl)phenyl]-N'-thiophen-3-ylurea
CAS No.:935660-78-9
Molecular Formula:C₁₇H₂₁BN₂O₃S
Molecular Weight:344.242
Hs Code.:

Synonyms:N-[4-(4,4,5,5-tetramethyl-[1,3,2]-dioxaborolan-2-yl)phenyl]-N'-thiophen-3-ylurea

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Chemical Property of N-[4-(4,4,5,5-tetramethyl-[1,3,2]-dioxaborolan-2-yl)phenyl]-N'-thiophen-3-ylurea

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Technology Process of N-[4-(4,4,5,5-tetramethyl-[1,3,2]-dioxaborolan-2-yl)phenyl]-N'-thiophen-3-ylurea

There total 2 articles about N-[4-(4,4,5,5-tetramethyl-[1,3,2]-dioxaborolan-2-yl)phenyl]-N'-thiophen-3-ylurea which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 76536-95-3
3-isocyanatothiophene

: 214360-73-3
4-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)aniline

: 935660-78-9
N-[4-(4,4,5,5-tetramethyl-[1,3,2]-dioxaborolan-2-yl)phenyl]-N'-thiophen-3-ylurea

Guidance literature:: With 4-methyl-morpholine; In tetrahydrofuran;
DOI:10.1016/j.bmcl.2006.12.015

Reference yield:

: 2-(4-isocyanatophenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

: 17721-06-1
3-aminothiophene

: 935660-78-9
N-[4-(4,4,5,5-tetramethyl-[1,3,2]-dioxaborolan-2-yl)phenyl]-N'-thiophen-3-ylurea

Guidance literature:: In dichloromethane; at 0 - 20 ℃;
DOI:10.1021/jm061280h

Reference yield:

: 935660-78-9
N-[4-(4,4,5,5-tetramethyl-[1,3,2]-dioxaborolan-2-yl)phenyl]-N'-thiophen-3-ylurea

: 599191-73-8
4-iodine-1H-indazol-3-ylamine

: C₁₈H₁₅N₅OS

Guidance literature:: With sodium carbonate; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; In 1,2-dimethoxyethane; water; at 85 ℃; for 16h;
DOI:10.1021/jm061280h