(S)-tert-butyl 1-(2-amino-4-(trifluoromethyl)phenoxy)-3-methylbutan-2-ylcarbamate

Base Information

Chemical Name:(S)-tert-butyl 1-(2-amino-4-(trifluoromethyl)phenoxy)-3-methylbutan-2-ylcarbamate
CAS No.:1073176-42-7
Molecular Formula:C₁₇H₂₅F₃N₂O₃
Molecular Weight:362.392
Hs Code.:

Synonyms:(S)-tert-butyl 1-(2-amino-4-(trifluoromethyl)phenoxy)-3-methylbutan-2-ylcarbamate

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Chemical Property of (S)-tert-butyl 1-(2-amino-4-(trifluoromethyl)phenoxy)-3-methylbutan-2-ylcarbamate

Chemical Property:

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Technology Process of (S)-tert-butyl 1-(2-amino-4-(trifluoromethyl)phenoxy)-3-methylbutan-2-ylcarbamate

There total 1 articles about (S)-tert-butyl 1-(2-amino-4-(trifluoromethyl)phenoxy)-3-methylbutan-2-ylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 1073176-29-0
(S)-tert-butyl 3-methyl-1-(2-nitro-4-(trifluoromethyl)phenoxy)butan-2-ylcarbamate

: 1073176-42-7
(S)-tert-butyl 1-(2-amino-4-(trifluoromethyl)phenoxy)-3-methylbutan-2-ylcarbamate

Guidance literature:: With 10% Pd/C; ammonium formate; In methanol; ethyl acetate; at 50 ℃; for 2h;
DOI:10.1002/anie.200802648

Reference yield: 97.0%

: 1073176-42-7
(S)-tert-butyl 1-(2-amino-4-(trifluoromethyl)phenoxy)-3-methylbutan-2-ylcarbamate

: 108-24-7
acetic anhydride

: 1073176-44-9
(S)-tert-butyl 1-(2-ethanamido-4-(trifluoromethyl)phenoxy)-3-methylbutan-2-ylcarbamate

Guidance literature:: With pyridine; dmap; at 0 ℃;
DOI:10.1002/anie.200802648

Reference yield: 93.0%

: 1073176-42-7
(S)-tert-butyl 1-(2-amino-4-(trifluoromethyl)phenoxy)-3-methylbutan-2-ylcarbamate

: 109-90-0
ethyl isocyanate

: 1402743-71-8
C₁₅H₂₂F₃N₃O₂

Guidance literature:: (S)-tert-butyl 1-(2-amino-4-(trifluoromethyl)phenoxy)-3-methylbutan-2-ylcarbamate; ethyl isocyanate; In tetrahydrofuran; dichloromethane; at 20 ℃; for 0.75h;

With trifluoroacetic acid; In tetrahydrofuran; dichloromethane; at 0 - 20 ℃;
DOI:10.1002/anie.201203852