2,4,6-tri-O-benzoyl-β-D-galactopyranosyl-(1-> 4)-1,2,3,6-tetra-O-benzoyl-α,β-D-glycopyranose

Base Information

Chemical Name:2,4,6-tri-O-benzoyl-β-D-galactopyranosyl-(1-> 4)-1,2,3,6-tetra-O-benzoyl-α,β-D-glycopyranose
CAS No.:359669-34-4
Molecular Formula:C₆₁H₅₀O₁₈
Molecular Weight:1071.06
Hs Code.:

Synonyms:2,4,6-tri-O-benzoyl-β-D-galactopyranosyl-(1-> 4)-1,2,3,6-tetra-O-benzoyl-α,β-D-glycopyranose

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Chemical Property of 2,4,6-tri-O-benzoyl-β-D-galactopyranosyl-(1-> 4)-1,2,3,6-tetra-O-benzoyl-α,β-D-glycopyranose

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Technology Process of 2,4,6-tri-O-benzoyl-β-D-galactopyranosyl-(1-> 4)-1,2,3,6-tetra-O-benzoyl-α,β-D-glycopyranose

There total 1 articles about 2,4,6-tri-O-benzoyl-β-D-galactopyranosyl-(1-> 4)-1,2,3,6-tetra-O-benzoyl-α,β-D-glycopyranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 1663-61-2
triethoxymethylbenzene

: C₅₄H₄₆O₁₇

: 359669-34-4
2,4,6-tri-O-benzoyl-β-D-galactopyranosyl-(1-> 4)-1,2,3,6-tetra-O-benzoyl-α,β-D-glycopyranose

Guidance literature:: triethoxymethylbenzene; C₅₄H₄₆O₁₇; With toluene-4-sulfonic acid; In dichloromethane; benzene; at 60 ℃; for 48h;

With acetic acid; In water; at 20 ℃; for 3h;
DOI:10.1016/S0008-6215(01)00097-0

Reference yield: 100.0%

: 108-24-7
acetic anhydride

: 359669-34-4
2,4,6-tri-O-benzoyl-β-D-galactopyranosyl-(1-> 4)-1,2,3,6-tetra-O-benzoyl-α,β-D-glycopyranose

: 359669-36-6
C₆₃H₅₂O₁₉

Guidance literature:: With pyridine; at 20 ℃; for 20h;
DOI:10.1016/S0008-6215(01)00097-0

Reference yield:

: 359669-34-4
2,4,6-tri-O-benzoyl-β-D-galactopyranosyl-(1-> 4)-1,2,3,6-tetra-O-benzoyl-α,β-D-glycopyranose

: 359669-38-8
C₅₆H₄₇BrO₁₇

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / pyridine / 20 h / 20 °C

2: 96 percent / HBr / CH₂Cl₂; acetic acid / 1 h / 0 - 20 °C

With pyridine; hydrogen bromide; In dichloromethane; acetic acid;
DOI:10.1016/S0008-6215(01)00097-0