2-(1-benzyl-1H-1,2,3-triazol-4-yl)-1-(4-(phenylsulfonyl)phenyl)ethanol

Base Information

Chemical Name:2-(1-benzyl-1H-1,2,3-triazol-4-yl)-1-(4-(phenylsulfonyl)phenyl)ethanol
CAS No.:1621085-05-9
Molecular Formula:C₂₃H₂₁N₃O₃S
Molecular Weight:419.504
Hs Code.:

Synonyms:2-(1-benzyl-1H-1,2,3-triazol-4-yl)-1-(4-(phenylsulfonyl)phenyl)ethanol

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Chemical Property of 2-(1-benzyl-1H-1,2,3-triazol-4-yl)-1-(4-(phenylsulfonyl)phenyl)ethanol

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Technology Process of 2-(1-benzyl-1H-1,2,3-triazol-4-yl)-1-(4-(phenylsulfonyl)phenyl)ethanol

There total 2 articles about 2-(1-benzyl-1H-1,2,3-triazol-4-yl)-1-(4-(phenylsulfonyl)phenyl)ethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 1621085-03-7
1-(4-(phenylsulfonyl)phenyl)but-3-yn-1-ol

: 622-79-7
benzyl azide

: 1621085-05-9
2-(1-benzyl-1H-1,2,3-triazol-4-yl)-1-(4-(phenylsulfonyl)phenyl)ethanol

Guidance literature:: With copper(ll) sulfate pentahydrate; sodium L-ascorbate; In water; tert-butyl alcohol; at 25 - 30 ℃; for 0.333333h; Sonication; Green chemistry;
DOI:10.1016/j.ejmech.2014.07.042

Reference yield:

: 66-39-7
4-(phenylsulfonyl)benzaldehyde

: 1621085-05-9
2-(1-benzyl-1H-1,2,3-triazol-4-yl)-1-(4-(phenylsulfonyl)phenyl)ethanol

Guidance literature:: Multi-step reaction with 2 steps

1: zinc; zinc dibromide / tetrahydrofuran / 1 h / 25 - 30 °C / Sonication

2: copper(ll) sulfate pentahydrate; sodium L-ascorbate / water; tert-butyl alcohol / 0.33 h / 25 - 30 °C / Sonication; Green chemistry

With copper(ll) sulfate pentahydrate; sodium L-ascorbate; zinc dibromide; zinc; In tetrahydrofuran; water; tert-butyl alcohol; 1: |Barbier Coupling Reaction;
DOI:10.1016/j.ejmech.2014.07.042

Reference yield: 80.0%

: 1621085-05-9
2-(1-benzyl-1H-1,2,3-triazol-4-yl)-1-(4-(phenylsulfonyl)phenyl)ethanol

: 106-96-7
propargyl bromide

: 1621085-07-1
1-benzyl-4-(2-(4-(phenylsulfonyl)phenyl)-2-(prop-2-yn-1-yloxy)ethyl)-1H-1,2,3-triazole

Guidance literature:: 2-(1-benzyl-1H-1,2,3-triazol-4-yl)-1-(4-(phenylsulfonyl)phenyl)ethanol; With sodium hydride; In N,N-dimethyl-formamide; at -20 ℃;

propargyl bromide; In N,N-dimethyl-formamide; at -20 ℃; for 0.5h; Sonication;
DOI:10.1016/j.ejmech.2014.07.042