4-methyl-N-((E)-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)allyl)-N-((Z)-4-(((E)-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)allyl)oxy)but-2-en-1-yl)-benzenesulfonamide

Base Information

Chemical Name:4-methyl-N-((E)-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)allyl)-N-((Z)-4-(((E)-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)allyl)oxy)but-2-en-1-yl)-benzenesulfonamide
CAS No.:1393589-93-9
Molecular Formula:C₂₉H₄₅B₂NO₇S
Molecular Weight:573.367
Hs Code.:

4-methyl-N-((E)-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)allyl)-N-((Z)-4-(((E)-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)allyl)oxy)but-2-en-1-yl)-benzenesulfonamide

Synonyms:4-methyl-N-((E)-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)allyl)-N-((Z)-4-(((E)-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)allyl)oxy)but-2-en-1-yl)-benzenesulfonamide

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Chemical Property of 4-methyl-N-((E)-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)allyl)-N-((Z)-4-(((E)-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)allyl)oxy)but-2-en-1-yl)-benzenesulfonamide

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Technology Process of 4-methyl-N-((E)-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)allyl)-N-((Z)-4-(((E)-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)allyl)oxy)but-2-en-1-yl)-benzenesulfonamide

There total 4 articles about 4-methyl-N-((E)-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)allyl)-N-((Z)-4-(((E)-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)allyl)oxy)but-2-en-1-yl)-benzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 1393589-92-8
(Z)-4-methyl-N-(prop-2-yn-1-yl)-N-(4-(prop-2-yn-1-yloxy)but-2-en-1-yl)-benzenesulfonamide

: 25015-63-8
4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane

: 1393589-93-9
4-methyl-N-((E)-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)allyl)-N-((Z)-4-(((E)-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)allyl)oxy)but-2-en-1-yl)-benzenesulfonamide

Guidance literature:: (Z)-4-methyl-N-(prop-2-yn-1-yl)-N-(4-(prop-2-yn-1-yloxy)but-2-en-1-yl)-benzenesulfonamide; 4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane; With triethylamine; at 0 ℃; for 0.0833333h; Inert atmosphere;

With Schwartz's reagent; at 60 ℃; for 16h; Inert atmosphere;
DOI:10.1021/ol3020623

Reference yield:

: 55022-46-3
4-methyl-N-prop-2-ynylbenzenesulfonamide

: 1393589-93-9
4-methyl-N-((E)-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)allyl)-N-((Z)-4-(((E)-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)allyl)oxy)but-2-en-1-yl)-benzenesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 36 h / 0 - 20 °C / Inert atmosphere

2.1: triethylamine / 0.08 h / 0 °C / Inert atmosphere

2.2: 16 h / 60 °C / Inert atmosphere

With di-isopropyl azodicarboxylate; triethylamine; triphenylphosphine; In tetrahydrofuran;
DOI:10.1021/ol3020623

Reference yield:

: 98-59-9
p-toluenesulfonyl chloride

: 1393589-93-9
4-methyl-N-((E)-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)allyl)-N-((Z)-4-(((E)-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)allyl)oxy)but-2-en-1-yl)-benzenesulfonamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: dmap; triethylamine / dichloromethane / 18.5 h / 0 - 20 °C / Inert atmosphere

2.1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 36 h / 0 - 20 °C / Inert atmosphere

3.1: triethylamine / 0.08 h / 0 °C / Inert atmosphere

3.2: 16 h / 60 °C / Inert atmosphere

With dmap; di-isopropyl azodicarboxylate; triethylamine; triphenylphosphine; In tetrahydrofuran; dichloromethane;
DOI:10.1021/ol3020623