(2R,4S,6R)-3-(benzyloxy)-7-(tert-butyldiphenylsilyloxy)-2,4,6-trimethylheptanal

Base Information

Chemical Name:(2R,4S,6R)-3-(benzyloxy)-7-(tert-butyldiphenylsilyloxy)-2,4,6-trimethylheptanal
CAS No.:1228007-29-1
Molecular Formula:C₃₃H₄₄O₃Si
Molecular Weight:516.796
Hs Code.:

Synonyms:(2R,4S,6R)-3-(benzyloxy)-7-(tert-butyldiphenylsilyloxy)-2,4,6-trimethylheptanal

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2R,4S,6R)-3-(benzyloxy)-7-(tert-butyldiphenylsilyloxy)-2,4,6-trimethylheptanal

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Technology Process of (2R,4S,6R)-3-(benzyloxy)-7-(tert-butyldiphenylsilyloxy)-2,4,6-trimethylheptanal

There total 1 articles about (2R,4S,6R)-3-(benzyloxy)-7-(tert-butyldiphenylsilyloxy)-2,4,6-trimethylheptanal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 1228007-28-0
(2S,4S,6R)-3-(benzyloxy)-7-(tert-butyldiphenylsilyloxy)-2,4,6-trimethylheptan-1-ol

: 1228007-29-1
(2R,4S,6R)-3-(benzyloxy)-7-(tert-butyldiphenylsilyloxy)-2,4,6-trimethylheptanal

Guidance literature:: With sodium hydrogencarbonate; Dess-Martin periodane; In dichloromethane; at 0 ℃; for 1h;
DOI:10.1002/ejoc.200901448

Reference yield: 76.0%

: 1228007-29-1
(2R,4S,6R)-3-(benzyloxy)-7-(tert-butyldiphenylsilyloxy)-2,4,6-trimethylheptanal

: 3020-28-8
(iodomethyl)triphenylphosphonium iodide

: 1228007-19-9
(2R,4S,5R,6S,Z)-5-((benzyloxy)-8-iodo-2,4,6-trimethyloct-7-enyloxy)tert-butyldiphenylsilane

Guidance literature:: (iodomethyl)triphenylphosphonium iodide; With sodium hexamethyldisilazane; In tetrahydrofuran; at 20 ℃; for 0.333333h; Inert atmosphere;

(2R,4S,6R)-3-(benzyloxy)-7-(tert-butyldiphenylsilyloxy)-2,4,6-trimethylheptanal; With N,N,N,N,N,N-hexamethylphosphoric triamide; In tetrahydrofuran; at -78 ℃; for 1h; Inert atmosphere;
DOI:10.1002/ejoc.200901448