Diphenylphosphinothioyl bromide

Base Information

• Chemical Name: Diphenylphosphinothioyl bromide
• CAS No.: 16534-67-1
• Molecular Formula: C₁₂H₁₀BrPS
• Molecular Weight: 297.155

Synonyms:Diphenylphosphinothioyl bromide

Chemical Property of Diphenylphosphinothioyl bromide

Chemical Property:

Purity/Quality:

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Technology Process of Diphenylphosphinothioyl bromide

There total 1 articles about Diphenylphosphinothioyl bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

→ Diphenylphosphinothioyl bromide (16534-67-1)

Guidance literature:

PSBr3, 2Mol AlBr3, 1Mol Bzl. bei 85grad; in geringer Menge neben Phenyl-thiophosphonsaeuredibromid;

DOI:10.1002/hlca.19640470115

Reference yield: 86.0%

Diphenylphosphinothioyl bromide (16534-67-1) + uridine (58-96-8) → Uridine-2',3',5'-O-tris-diphenylphosphinothioate (74334-87-5)

Guidance literature:

With pyridine; at 5 ℃; for 4h;

Reference yield: 71.0%

Diphenylphosphinothioyl bromide (16534-67-1) + 2',3'-isopropylidene adenosine (362-75-4) → 2',3'-O-Isopropylidene-5'-O-diphenylphosphinothioyladenosine (74334-88-6)

Guidance literature:

With pyridine; 1) 5 deg C, 4 h 2) room temperature, 2 h;

Downstream raw materials:

2',3'-O-Isopropylidene-5'-O-diphenylphosphinothioyladenosine

Uridine-2',3',5'-O-tris-diphenylphosphinothioate

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